苄基 4,6-O-亚苄基-alpha-D-吡喃甘露糖苷合成路线 （共 12 条）
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=80°C; 2.5 h; Inert atmosphere;
参考文献
Zheng, Shaojun; Laraia, Luca; O'Connor, Cornelius J.; Sorrell, David; Tan, Yaw Sing; Xu, Zhaochao; Venkitaraman, Ashok R.; Wu, Wenjun; Spring, David R.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2590 - 2593
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; water; ethyl acetate 7 h; Heating;
参考文献
Fuegedi, Peter; Liptak, Andras; Nanasi, Pal; Szejtli, Jozsef
Carbohydrate Research, 1982 , vol. 104, p. 55 - 68
反应条件
toluene-4-sulfonic acid in acetonitrile 1.25 h; Ambient temperature;
参考文献
Magnusson, Goeran; Ahlfors, Stefan; Dahmen, Jan; Jansson, Karl; Nilsson, Ulf; et al.
Journal of Organic Chemistry, 1990 , vol. 55, # 12 p. 3932 - 3946
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 24 h / 20 °C / Inert atmosphere 2: methanol; water; triethylamine / 5 h / Inert atmosphere 3: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 2.5 h / 80 °C / Inert atmosphere View Scheme
参考文献
University of Iowa Research Foundation; Kraus, George A.; Maury, Wendy
Patent: US2013/252909 A1, 2013 ;
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 24 h / 20 °C / Inert atmosphere 2: methanol; water; triethylamine / 5 h / Inert atmosphere 3: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 2.5 h / 80 °C / Inert atmosphere View Scheme
参考文献
University of Iowa Research Foundation; Kraus, George A.; Maury, Wendy
Patent: US2013/252909 A1, 2013 ;
反应条件
1: sodium methoxide / methanol 2: toluene-p-sulfonic acid monohydrate / 4 h / Ambient temperature View Scheme
参考文献
University of Iowa Research Foundation; Kraus, George A.; Maury, Wendy
Patent: US2013/252909 A1, 2013 ;
反应条件
1: 49 percent / M sodium methoxide, zinc chloride / methanol; CHCl3 2: 14 percent / lithium aluminium hydride / tetrahydrofuran; H2O; ethyl acetate / 7 h / Heating View Scheme
参考文献
Fuegedi, Peter; Liptak, Andras; Nanasi, Pal; Szejtli, Jozsef
Carbohydrate Research, 1982 , vol. 104, p. 55 - 68
反应条件
1: 49 percent / M sodium methoxide, zinc chloride / methanol; CHCl3 2: 14 percent / lithium aluminium hydride / tetrahydrofuran; H2O; ethyl acetate / 7 h / Heating View Scheme
参考文献
Fuegedi, Peter; Liptak, Andras; Nanasi, Pal; Szejtli, Jozsef
Carbohydrate Research, 1982 , vol. 104, p. 55 - 68
反应条件
1: 76 percent / mercuric oxide, mercuric bromide, drierite, calcium carbonate / CH2Cl2 2: 49 percent / M sodium methoxide, zinc chloride / methanol; CHCl3 3: 14 percent / lithium aluminium hydride / tetrahydrofuran; H2O; ethyl acetate / 7 h / Heating View Scheme
参考文献
Fuegedi, Peter; Liptak, Andras; Nanasi, Pal; Szejtli, Jozsef
Carbohydrate Research, 1982 , vol. 104, p. 55 - 68
反应条件
toluene-4-sulfonic acid 4 h; Ambient temperature;
参考文献
Hoffman, James; Theander, Olof; Lindberg, Mats; Norberg, Thomas
Carbohydrate Research, 1985 , vol. 137, p. 265 - 269
