N-羟基-alpha-苯基-苯乙酰胺合成路线 （共 13 条）
反应条件
1: With carbonyl diimidazole in acetonitrile T=20°C; Lossen rearrangement; 0.5 h; Inert atmosphere; 2: in acetonitrile T=60°C; Lossen rearrangement; Inert atmosphere;
参考文献
Yoganathan, Sabesan; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 3 p. 602 - 605
反应条件
1: SOCl2; DMF
2: hydroxylamine; Et3N / H2O; tetrahydrofuran
View Scheme
参考文献
KrennHrubec, Keris; Marshall, Brett L.; Hedglin, Mark; Verdin, Eric; Ulrich, Scott M.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 10 p. 2874 - 2878
反应条件
hydroxylamine hydrochloride; sodium carbonate
参考文献
Jones; Hurd
Journal of the American Chemical Society, 1921 , vol. 43, p. 2433
反应条件
hydroxylamine; potassium cyanide in tetrahydrofuran; methanol; water
24 h;
参考文献
Boldt, Grant E.; Kennedy, Jack P.; Janda, Kim D.
Organic Letters, 2006 , vol. 8, # 8 p. 1729 - 1732
反应条件
hydroxylamine in water; acetonitrile
T=23°C; 14 h;
参考文献
Yoganathan, Sabesan; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 3 p. 602 - 605
反应条件
hydroxylamine; sodium methylate
参考文献
Jones; Hurd
Journal of the American Chemical Society, 1921 , vol. 43, p. 2433
反应条件
sodium acetate; acetic acid
参考文献
Hurd et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 4697
反应条件
acetic acid ester; diethyl ether; hydroxylamine; benzene
参考文献
Jones; Hurd
Journal of the American Chemical Society, 1921 , vol. 43, p. 2433
反应条件
1: AlCl3 / anschliessend mit wss. HCl behandeln
2: aqueous acetic acid; sodium acetate
View Scheme
参考文献
Hurd et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 4697
反应条件
1: AlCl3 / anschliessend mit wss. HCl behandeln
2: aqueous acetic acid; sodium acetate
View Scheme
参考文献
Hurd et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 4697
