2-碘-4,6-二甲基苯胺合成路线 （共 7 条）
反应条件
IPy2BF4 in dichloromethane T=20°C; Iodination; 0.0833333 h;
参考文献
Yang, Shyh-Chyun; Chung, Wen-Hung
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999 , vol. 38, # 8 p. 897 - 904
参考文献
Benda
Chemische Berichte, 1909 , vol. 42, p. 3622
反应条件
Einw. von 1 Mol.-Gew. Chlorjod;
参考文献
Kerschbaum
Chemische Berichte, 1895 , vol. 28, p. 2800
反应条件
Einw. von 2 Mol.-Gew. Chlorjod;
参考文献
Kerschbaum
Chemische Berichte, 1895 , vol. 28, p. 2800
反应条件
2Na(1+)*CuC6H4(NCHC6H3OO3S)2(2-)=CuC6H4(NCHC6H3ONaO3S)2; tetrabutylammomium bromide; potassium carbonate in water T=120°C; 30 h;
参考文献
Journal of Organometallic Chemistry, , vol. 705, p. 75 - 78
反应条件
1: 98 percent / Et3N / Pd(PPh3)2Cl2-CuI / 3 h / 0 - 20 °C
2: 82 percent / CuI / dimethylformamide / 2.5 h / 100 °C
View Scheme
参考文献
Ezquerra, Jesus; Pedregal, Concepcion; Lamas, Carlos; Barluenga, Jose; Perez, Marta; Garcia-Martin, Miguel Angel; Gonzalez, Jose M.
Journal of Organic Chemistry, 1996 , vol. 61, # 17 p. 5804 - 5812
反应条件
(i) NaNO2, H2SO4, (ii) aq. KI; Multistep reaction;
参考文献
Suzuki,H. et al.
Bulletin of the Chemical Society of Japan, 1965 , vol. 38, p. 1590 - 1595
