6-甲氧基-4-甲基喹啉水合物合成路线 （共 33 条）
反应条件
phospho-tungstic acid; phosphotungstic acid; silica gel Doebner-Miller reaction; 0.166667 h; microwave irradiation;
参考文献
Sivaprasad, Ganesabaskaran; Rajesh, Rengasamy; Perumal, Paramasivan T.
Tetrahedron Letters, 2006 , vol. 47, # 11 p. 1783 - 1785
反应条件
acetyl chloride in ethanol T=20 - 50°C; 1.16667 h;
参考文献
Kobayashi, Yuichi; Igarashi, Junji; Feng, Chao; Toshifumi; Tojo
Tetrahedron Letters, 2012 , vol. 53, # 29 p. 3742 - 3745
反应条件
sodium hydroxide in methanol T=50°C; 12 h;
参考文献
Theeraladanon, Chumpol; Arisawa, Mitsuhiro; Nishida, Atsushi; Nakagawa, Masako
Tetrahedron, 2004 , vol. 60, # 13 p. 3017 - 3035
反应条件
potassium hydroxide; ethanol; nickel T=60 - 70°C; Hydrogenation;
参考文献
Ainley; King
Pr. roy. Soc. <B>, 1938 , vol. 125, p. 60,84
反应条件
ruthenium trichloride; tributylphosphine; MgBr2*Et2O in 1,3,5-trimethyl-benzene 16 h; Inert atmosphereReflux;
参考文献
Monrad, Rune Nygaard; Madsen, Robert
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 610 - 615
反应条件
1: With sulfuric acid 2: With trichlorophosphate 3: With acetic acid; zinc Further stages.;
参考文献
Igarashi, Junji; Katsukawa, Masahiro; Wang, Yong-Gang; Acharya, Hukum P.; Kobayashi, Yuichi
Tetrahedron Letters, 2004 , vol. 45, # 19 p. 3783 - 3786
反应条件
ethanol; iron(III) chloride; zinc(II) chloride
参考文献
Campbell; Schaffner
Journal of the American Chemical Society, 1945 , vol. 67, p. 86,88
反应条件
ethanol; iron(III) chloride; zinc(II) chloride
参考文献
Campbell; Schaffner
Journal of the American Chemical Society, 1945 , vol. 67, p. 86,88
反应条件
hydrogenchloride; acetone Reagens 4: konz.Salzsaeure;
参考文献
Kobayashi, Yuichi; Igarashi, Junji; Feng, Chao; Toshifumi; Tojo
Tetrahedron Letters, 2012 , vol. 53, # 29 p. 3742 - 3745
反应条件
1: 88 percent / CH2Cl2 / 0.17 h / 0 °C 2: 70 percent / NaH / dimethylformamide / 1 h / 0 °C 3: 98 percent / Cl2Ru(PCy3)(=CHPh)(N,N'-(Mes)2-imidazolidin-2-yl) / CH2Cl2 / 1 h / 50 °C 4: 98 percent / aq. NaOH / methanol / 12 h / 50 °C View Scheme
参考文献
Theeraladanon, Chumpol; Arisawa, Mitsuhiro; Nishida, Atsushi; Nakagawa, Masako
Tetrahedron, 2004 , vol. 60, # 13 p. 3017 - 3035
