反应条件
in neat (no solvent)
byproducts: HgI2; CF3SiI:HgS molar ratio was 1:2, in a sealed tube, 300 K for 7 days, under dry N2; low temp. fractionated distn., less volatile fraction was purified by passing it through a 198 K trap into a trap held at 173 K, the (F3SiS)2SiF2 was identified by NMR, its purity was 98 percent;;
参考文献
Beckers, Helmut; Buerger, Hans
Zeitschrift fur Anorganische und Allgemeine Chemie, 2001 , vol. 627, # 6 p. 1217 - 1224
