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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
41067-80-5
合成路线
（共 16 条）
110-91-8
吗啉
+
452905-58-7
2,3,4,5,6-五氟-1-乙烯磺酸苯酯
→
反应条件
41067-80-5
反应条件
2-tert-butylimino-2-diethylamino-1,3-dimethylperhydro-1,3,2-diazaphosphorine in 1,4-dioxane T=0 - 22°C; 2 h;
参考文献
Bristol-Myers Squibb Company
Patent: US2007/275947 A1, 2007 ;
Location in patent: Page/Page column 35-36 ;
US 20070275947 A1
110-91-8
吗啉
+
1622-32-8
2-氯乙烷磺酰氯
→
反应条件
41067-80-5
反应条件
triethylamine in ethyl acetate T=0°C;
参考文献
Lonchambon, Georges; Delacroix, Alain; Petit, Jacques; Lecomte, Patrice
Bulletin de la Societe Chimique de France, 1981 , vol. 2, # 1-2 p. 71 - 74
41067-80-5
→
反应条件
173336-66-8
2-(吗啉-4-基磺酰基)乙胺盐酸盐
反应条件
ammonium hydroxide in methanol T=20°C;
参考文献
Shionogi and Co., Ltd.; YUKIMASA, Akira
Patent: WO2012/144661 A1, 2012 ;
Location in patent: Page/Page column 93 ;
WO 2012/144661 A1
41067-80-5
→
反应条件
87975-05-1
反应条件
1: 86 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 60 percent / triethylamine / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
41067-80-5
→
反应条件
87975-14-2
反应条件
1: 86 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 60 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 62 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
41067-80-5
→
反应条件
87975-15-3
反应条件
1: 86 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 60 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 61 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
41067-80-5
→
反应条件
87975-16-4
反应条件
1: 86 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 60 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 80 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
41067-80-5
→
反应条件
87975-17-5
反应条件
1: 86 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 60 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 80 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
41067-80-5
→
反应条件
87975-18-6
反应条件
1: 86 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 60 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 85 percent / benzene / 24 h / Ambient temperature View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
41067-80-5
→
反应条件
87975-39-1
反应条件
1: 86 percent / Br2 / CCl4 / 48 h / Ambient temperature 2: 60 percent / triethylamine / benzene / 24 h / Ambient temperature 3: 61 percent / dimethylsulfoxide / 4 h / 75 °C View Scheme
参考文献
Aumaitre, Guy; Chanet-Ray, Josette; Durand, Jacques; Vessiere, Roger; Lonchambon, Georges
Synthesis, 1983 , # 10 p. 816 - 821
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