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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
环丙基硼酸
合成路线
（共 67 条）
3430-22-6
4-甲基-3-溴吡啶
+
411235-57-9
环丙基硼酸
→
反应条件
1245643-68-8
反应条件
K3PO4*7H2O; C45H53ClFeNO2PPd in water; toluene T=100°C; Suzuki coupling; 8 h; Inert atmosphere;
参考文献
Zhang, Min; Cui, Xiuling; Chen, Xiaopei; Wang, Lianhui; Li, Jingya; Wu, Yusheng; Hou, Lifen; Wu, Yangjie
Tetrahedron, 2012 , vol. 68, # 3 p. 900 - 905
4175-77-3
2,4-二溴噻唑
+
411235-57-9
环丙基硼酸
→
反应条件
1086381-69-2
4-溴-2-环丙基-5-甲基噻唑
反应条件
potassium phosphate; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=80°C; Suzuki coupling; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Strotman, Neil A.; Chobanian, Harry R.; He, Jiafang; Guo, Yan; Dormer, Peter G.; Jones, Christina M.; Steves, Janelle E.
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1733 - 1739
55-21-0
苯甲酰胺
+
411235-57-9
环丙基硼酸
→
反应条件
15205-35-3
N-环丙基-苯甲酰胺
反应条件
4-(N,N-dimethlyamino)pyridine; air; copper diacetate; sodium hexamethyldisilazane in toluene T=95°C; 16 h; Inert atmosphere;
参考文献
Tsuritani, Takayuki; Strotman, Neil A.; Yamamoto, Yuhei; Kawasaki, Masashi; Yasuda, Nobuyoshi; Mase, Toshiaki
Organic Letters, 2008 , vol. 10, # 8 p. 1653 - 1655
→
反应条件
769159-85-5
4-环丙基-1-氟-2-硝基苯
反应条件
K3PO4*7H2O; C45H53ClFeNO2PPd in water; toluene T=100°C; Suzuki coupling; 10 h; Inert atmosphere;
参考文献
Zhang, Min; Cui, Xiuling; Chen, Xiaopei; Wang, Lianhui; Li, Jingya; Wu, Yusheng; Hou, Lifen; Wu, Yangjie
Tetrahedron, 2012 , vol. 68, # 3 p. 900 - 905
57260-71-6
1-Boc-哌嗪
+
411235-57-9
环丙基硼酸
→
反应条件
77278-34-3
1-环丙基哌嗪-4-羧酸叔丁酯
反应条件
[2,2']bipyridinyl; oxygen; copper diacetate; sodium carbonate in 1,2-dichloro-ethane T=70°C; Chan-Lam reaction;
参考文献
Benard, Sebastien; Neuville, Luc; Zhu, Jieping
Chemical Communications, 2010 , vol. 46, # 19 p. 3393 - 3395
939437-77-1
+
411235-57-9
环丙基硼酸
→
反应条件
870810-00-7
2-(4-溴-2-(1-(2,6-二氯苯基)-1H-吡唑-4-羰基)苯氧基)乙酸
+
939437-76-0
反应条件
sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=90°C; 120 h;
参考文献
7TM PHARMA A/S
Patent: WO2007/62678 A1, 2007 ;
Location in patent: Page/Page column 12-13 ;
WO 2007/062678 A1
656-64-4
3-溴-4-氟苯胺
+
411235-57-9
环丙基硼酸
→
反应条件
890129-90-5
3-环丙基-4-氟苯胺
反应条件
potassium phosphate; tri-cyclo-hexyl-phosphine; palladium diacetate in water; toluene T=100°C;
参考文献
Conte, Aurelia; Kuehne, Holger; Luebbers, Thomas; Mattei, Patrizio; Maugeais, Cyrille; Mueller, Werner; Pflieger, Philippe
Patent: US2007/185058 A1, 2007 ;
Location in patent: Page/Page column 13 ;
1072-97-5
+
411235-57-9
环丙基硼酸
→
反应条件
893738-68-6
反应条件
K3PO4*7H2O; C45H53ClFeNO2PPd in water; toluene T=100°C; Suzuki coupling; 6 h; Inert atmosphere;
参考文献
Zhang, Min; Cui, Xiuling; Chen, Xiaopei; Wang, Lianhui; Li, Jingya; Wu, Yusheng; Hou, Lifen; Wu, Yangjie
Tetrahedron, 2012 , vol. 68, # 3 p. 900 - 905
367-24-8
+
411235-57-9
环丙基硼酸
→
反应条件
893739-89-4
反应条件
potassium phosphate; palladium diacetate; tri-cyclo-hexyl-phosphine in water; toluene T=100°C; 48 h;
参考文献
Niu, Huifeng
Patent: US2008/207563 A1, 2008 ;
Location in patent: Page/Page column 50 ;
→
反应条件
900802-81-5
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate in tetrahydrofuran 16 h; Inert atmosphereReflux;
参考文献
PFIZER INC.; AHN, Kay; BOEHM, Markus; CABRAL, Shawn; CARPINO, Philip A.; FUTATSUGI, Kentaro; HEPWORTH, David; KUNG, Daniel W.; ORR, Suvi; WANG, Jian
Patent: WO2013/150416 A1, 2013 ;
Location in patent: Page/Page column 99 ;
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