1,3-二(苄亚基氨基)脲合成路线 （共 8 条）
反应条件
phosphonic acid diethyl ester; toluene-4-sulfonic acid hydrazide in dimethyl sulfoxide
T=60°C; 10 h;
参考文献
Wen, Jun; Yang, Chu-Ting; Jiang, Tao; Hu, Sheng; Yang, Tong-Zai; Wang, Xiao-Lin
Organic Letters, 2014 , vol. 16, # 9 p. 2398 - 2401
反应条件
phosphonic acid diethyl ester in dimethyl sulfoxide
T=60°C; 10 h; Reagent/catalystSolventTemperature;
参考文献
Wen, Jun; Yang, Chu-Ting; Jiang, Tao; Hu, Sheng; Yang, Tong-Zai; Wang, Xiao-Lin
Organic Letters, 2014 , vol. 16, # 9 p. 2398 - 2401
反应条件
in dimethyl sulfoxide
T=60°C; 10 h;
参考文献
Wen, Jun; Yang, Chu-Ting; Jiang, Tao; Hu, Sheng; Yang, Tong-Zai; Wang, Xiao-Lin
Organic Letters, 2014 , vol. 16, # 9 p. 2398 - 2401
参考文献
Li, Zheng; Zhu, Wei; Yu, Jinlan; Ma, Xuelin; Lu, Zhong; Xiao, Shuxiu
Synthetic Communications, 2006 , vol. 36, # 18 p. 2613 - 2619
反应条件
1: methanol / 1 h / |Reflux
2: phosphonic acid diethyl ester / dimethyl sulfoxide / 10 h / 60 °C
View Scheme
参考文献
Wen, Jun; Yang, Chu-Ting; Jiang, Tao; Hu, Sheng; Yang, Tong-Zai; Wang, Xiao-Lin
Organic Letters, 2014 , vol. 16, # 9 p. 2398 - 2401
参考文献
Curtius; Heidenreich
Journal fuer Praktische Chemie (Leipzig), 1895 , vol. <2>52, p. 476
Chemische Berichte, 1894 , vol. 27, p. 2685
参考文献
Brown; Pickering; Wilson
Journal of the Chemical Society, 1927 , p. 110
反应条件
1: sodium hydride / tetrahydrofuran / 2 h / Reflux
2: methanol; carbonic acid dihydrazide; toluene-4-sulfonic acid / 1 h / 20 °C
View Scheme
参考文献
Bancerz, Matthew; Youn, Beom; Dacosta, Matthew V.; Georges, Michael K.
Journal of Organic Chemistry, 2012 , vol. 77, # 5 p. 2415 - 2421
