Dess-Martin periodane in dichloromethane
T=20°C; 2 h;
参考文献
Halim, Marlin; Tremblay, Matthew S.; Jockusch, Steffen; Turro, Nicholas J.; Sames, Dalibor
Journal of the American Chemical Society, 2007 , vol. 129, # 25 p. 7704 - 7705
Aitken, R. Alan; Herion, Hugues; Janosi, Amaya; Karodia, Nazira; Raut, Swati V.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2467 - 2472
1.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 1 h / -78 °C
1.2: 65 percent / tetrahydrofuran / 2 h / -78 °C
2.1: 96 percent / Dess-Martin periodinane / CH2Cl2 / 2 h / 20 °C
View Scheme
参考文献
Halim, Marlin; Tremblay, Matthew S.; Jockusch, Steffen; Turro, Nicholas J.; Sames, Dalibor
Journal of the American Chemical Society, 2007 , vol. 129, # 25 p. 7704 - 7705
1: 68 percent / Et3N / toluene / 3 h / Ambient temperature
2: 67 percent / 3.5 h / 500 °C / 0 - 0.1 Torr
View Scheme
参考文献
Aitken, R. Alan; Herion, Hugues; Janosi, Amaya; Karodia, Nazira; Raut, Swati V.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2467 - 2472
1: 87 percent / Et3N / toluene / 3 h / Ambient temperature
2: 23 percent Spectr. / 1 h / 500 °C / 0 - 0.1 Torr
View Scheme
参考文献
Aitken, R. Alan; Herion, Hugues; Janosi, Amaya; Karodia, Nazira; Raut, Swati V.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2467 - 2472
