N-(4-溴苯基)丁二酰亚胺合成路线 (共 10 条)
反应条件
hydrazine hydrate in ethanol 20 h; Heating; Yield given;
参考文献
Tetrahedron Letters, , vol. 38, # 15 p. 2617 - 2620
反应条件
Bei der elektrochemischen Reduktion.;
参考文献
Smith; Merits
Fysiograf.Saellsk.Lund Foerh., 1953 , vol. 23, p. 88,90
反应条件
bis-triphenylphosphine-palladium(II) chloride; 4-bromooctafluorobutanetriethoxysilane; (Z)-N,N-diisopropyl-2-styrylbenzamide in tetrahydrofuran
T=65°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Bai, Xing-Feng; Xu, Li-Wen; Zheng, Long-Sheng; Jiang, Jian-Xiong; Lai, Guo-Qiao; Shang, Jun-Yan
Chemistry - A European Journal, 2012 , vol. 18, # 26 p. 8174 - 8179
反应条件
0.333333 h; Heating;
参考文献
Makurina, V. I.; Chuvurin, A. V.; Karnozhitskaya, T. M.; Chernykh, V. P.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 11 p. 1978 - 1980
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 11 p. 2290 - 2294
反应条件
1: acetic acid / 45 °C
2: sulfuric acid / 60 °C
View Scheme
参考文献
Patil, Sambhaji V.; Mahale, Keshao A.; Gosavi, Kirankumar S.; Deshmukh, Ganesh B.; Patil, Nilesh S.
Organic Preparations and Procedures International, 2013 , vol. 45, # 4 p. 314 - 320
反应条件
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in N,N-dimethyl-formamide
T=100°C; 0.5 h;
参考文献
Kumar, Padam Praveen; Reddy, Y. Dathu; Kumari, Y. Bharathi; Devi, B. Rama; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 4 p. 392 - 398
反应条件
hydrogenchloride in tetrahydrofuran
0.166667 h; Ambient temperature;
参考文献
Martin, Stephen F.; Limberakis, Chris
Tetrahedron Letters, 1997 , vol. 38, # 15 p. 2617 - 2620
反应条件
tetrabutylammomium bromide in neat (no solvent, solid phase)
MillingGreen chemistry;
参考文献
Kumar, Padam Praveen; Rama Devi; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 8 p. 1166 - 1171
反应条件
methanol; potassium cyanide; tetrabutyl ammonium fluoride
2.) 3 d; Yield givenMultistep reaction;
参考文献
Far; Tidwell
Journal of Organic Chemistry, 1998 , vol. 63, # 24 p. 8636 - 8637
反应条件
acetyl chloride
1.) benzene, reflux; 2.) reflux, 1 h; Yield given. Multistep reaction;
参考文献
Martin, Stephen F.; Limberakis, Chris
Tetrahedron Letters, 1997 , vol. 38, # 15 p. 2617 - 2620