1: With magnesium; ethylene dibromide in tetrahydrofuran T=20°C; Inert atmosphere; 2: With phosphorus trichoride in tetrahydrofuran Inert atmosphereCooling;
参考文献
Nawara-Hultzsch, Agnieszka J.; Skopek, Katrin; Shima, Takanori; Barbasiewicz, Micha; Hess, Gisela D.; Skaper, Dirk; Gladysz, John A.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2010 , vol. 65, # 3 p. 414 - 424
1: 6-heptenyl bromide With magnesium in tetrahydrofuran
2: With copper(l) iodide; methyllithium in tetrahydrofuran; diethyl ether
T=-78 - 10°C;
3: I(CH2)10COOMe in tetrahydrofuran; diethyl ether
T=-78 - 20°C; Further stages.;
参考文献
Rezanka, Tomas; Sigler, Karel
Phytochemistry, 2007 , vol. 68, # 6 p. 925 - 934
1: With magnesium; ethylene dibromide in tetrahydrofuran
T=20°C; Inert atmosphere;
2: With phosphorus trichoride in tetrahydrofuran
Inert atmosphereCooling;
参考文献
Nawara-Hultzsch, Agnieszka J.; Skopek, Katrin; Shima, Takanori; Barbasiewicz, Micha; Hess, Gisela D.; Skaper, Dirk; Gladysz, John A.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2010 , vol. 65, # 3 p. 414 - 424