1,4,8,11-四甲基-1,4,8,11-四氮杂-环一十四烷合成路线 （共 14 条）
反应条件
sodium hydroxide; formaldehyd; formic acid in water
参考文献
Murphy, Michael A; Malachowski, Mitchell R
Patent: US2005/85555 A1, 2005 ;
US 20050085555 A1
反应条件
potassium hydroxide; C14H30N2O4 in toluene 4 h; Ambient temperatureIrradiation;
参考文献
Jurczak, Janusz; Ostaszewski, Ryszard
Tetrahedron Letters, 1988 , vol. 29, # 8 p. 959 - 960
反应条件
1: 90 percent / acetonitrile / 2 h / 20 °C 2: 90 percent / NaBH4 / ethanol; H2O / 4 h / Heating View Scheme
参考文献
Royal, Guy; Dahaoui-Gindrey, Valerie; Dahaoui, Slimane; Tabard, Alain; Guilard, Roger; Pullumbi, Pluton; Lecomte, Claude
European Journal of Organic Chemistry, 1998 , # 9 p. 1971 - 1975
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Tang, Hui
Organometallics, 2000 , vol. 19, # 23 p. 4810 - 4819
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Tang, Hui
Organometallics, 2000 , vol. 19, # 23 p. 4810 - 4819
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Tang, Hui
Organometallics, 2000 , vol. 19, # 23 p. 4810 - 4819
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Tang, Hui
Organometallics, 2000 , vol. 19, # 23 p. 4810 - 4819
反应条件
1: With formic acid 24 h; Reflux; 2: With sodium hydroxide pH=> 12;
参考文献
Evangelio, Emi; Rath, Nigam P.; Mirica, Liviu M.
Dalton Transactions, 2012 , vol. 41, # 26 p. 8010 - 8021
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Tang, Hui
Organometallics, 2000 , vol. 19, # 23 p. 4810 - 4819
反应条件
in benzene-d6 stirred for a few min, left standing in NMR tube at 22°C for several h; reversible reaction; not isolated; (1)H NMR spectral data;
参考文献
Tang, Hui
Organometallics, 2000 , vol. 19, # 23 p. 4810 - 4819
