反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1749700', constants.ctx, '0')">ethyl 4-bromobutanoate</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '3587194', constants.ctx, '0')">iodine</a>; <a href="#" onclick="return RXDsubstances(event, this, '8973685', constants.ctx, '0')">zinc</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=80°C; 4.00833 h; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '2076973', constants.ctx, '0')">1-ethyl-4-iodobenzene</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '11411681', constants.ctx, '0')">NiCl<sub>2</sub>((PPh<sub>3</sub>)P)<sub>2</sub></a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=30 - 45°C; 80 h; <br /> <br />
参考文献
EMISPHERE TECHNOLOGIES, INC. Patent: WO2008/112368 A2, 2008 ; Location in patent: Page/Page column 38 ;
