N-苄氧羰基-L-谷氨酸酐合成路线 （共 62 条）
反应条件
hydrogenchloride; bis(1,5-cyclooctadiene)nickel (0); N,N,N',N,-tetramethylethylenediamine 1.) THF, reflux, 2.5h. (or tricyclohexylphosphine instead of N,N,N',N'-tetramethylethylenediamine); Yield given. Multistep reaction;
参考文献
Castano; Echavarren
Tetrahedron Letters, 1990 , vol. 31, # 33 p. 4783 - 4786
反应条件
hydrogenchloride; bis(1,5-cyclooctadiene)nickel (0); 2,9-dimethyl-1,10-phenanthroline 1.) THF, reflux, 2.5h.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Castano; Echavarren
Tetrahedron Letters, 1990 , vol. 31, # 33 p. 4783 - 4786
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0°C; 1 h; without DMAP; Yields of byproduct given;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
参考文献
Klieger,E.; Gibian,H.
Justus Liebigs Annalen der Chemie, 1962 , vol. 655, p. 195 - 210
Full Text Show Details
Le Quesne; Young
Journal of the Chemical Society, 1950 , p. 1954,1958
反应条件
pyridine in chloroform
参考文献
Goldschmidt,S. et al.
Chemische Berichte, 1964 , vol. 97, p. 2434 - 2438
反应条件
benzyl alcohol T=100°C;
参考文献
Bergmann; Zervas; Salzmann
Chemische Berichte, 1933 , vol. 66, p. 1288,1290
反应条件
1: ethyl acetate; NaHCO3; H2O 2: Hydrogenation View Scheme
参考文献
Sachs; Brand
Journal of the American Chemical Society, 1954 , vol. 76, p. 1815
反应条件
hydrogenchloride; bis(1,5-cyclooctadiene)nickel (0); N,N,N',N,-tetramethylethylenediamine 1.) THF, reflux, 2.5h. (or tricyclohexylphosphine instead of N,N,N',N'-tetramethylethylenediamine); Yield given. Multistep reaction;
参考文献
Castano; Echavarren
Tetrahedron Letters, 1990 , vol. 31, # 33 p. 4783 - 4786
反应条件
hydrogenchloride; bis(1,5-cyclooctadiene)nickel (0); 2,9-dimethyl-1,10-phenanthroline 1.) THF, reflux, 2.5h.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Castano; Echavarren
Tetrahedron Letters, 1990 , vol. 31, # 33 p. 4783 - 4786
反应条件
palladium on activated charcoal; acetic acid Hydrogenation;
参考文献
Hanby et al.
Journal of the Chemical Society, 1950 , p. 3239,3243
Full Text Show Details
Int. Minerals and Chem. Corp.
Patent: DE1015436 , 1954 ;
