N-苄氧羰基-L-谷氨酸酐合成路线 （共 62 条）
反应条件
1: in tetrahydrofuran T=-78°C; 4 h; 2: With citric acid in tetrahydrofuran
参考文献
Deguest, Geoffrey; Bischoff, Laurent; Fruit, Corinne; Marsais, Francis
Tetrahedron Asymmetry, 2006 , vol. 17, # 14 p. 2120 - 2125
反应条件
1: in tetrahydrofuran T=-78 - 20°C; 2: With citric acid in tetrahydrofuran
参考文献
Deguest, Geoffrey; Bischoff, Laurent; Fruit, Corinne; Marsais, Francis
Tetrahedron Asymmetry, 2006 , vol. 17, # 14 p. 2120 - 2125
反应条件
1: in tetrahydrofuran T=-78°C; 4 h; 2: With citric acid in tetrahydrofuran
参考文献
Deguest, Geoffrey; Bischoff, Laurent; Fruit, Corinne; Marsais, Francis
Tetrahedron Asymmetry, 2006 , vol. 17, # 14 p. 2120 - 2125
反应条件
anschliessendes Hydrieren;
参考文献
Matsukawa; Masuda
Yakugaku Zasshi, 1953 , vol. 73, p. 397
Chem.Abstr., 1954 , p. 2597
参考文献
Bergmann; Zervas
Chemische Berichte, 1932 , vol. 65, p. 1192,1198
Full Text Show Details
Melville
Biochemical Journal, 1935 , vol. 29, p. 179,182
反应条件
acetic anhydride
T=55°C; 0.5 h;
参考文献
Manesis, Nick J.; Goodman, Murray
Journal of Organic Chemistry, 1987 , vol. 52, # 24 p. 5331 - 5341
反应条件
1: 90 percent
2: 60 percent / dicyclohexylcarbodiimide / ethyl acetate / 1.) 1 h, 0 deg C, 2.) 24 h, r.t.
View Scheme
参考文献
Munegumi, Toratane; Meng, Yan-Quing; Harada, Kaoru
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 8 p. 2748 - 2750
反应条件
1: 90 percent
2: 60 percent / dicyclohexylcarbodiimide / ethyl acetate / 1.) 1 h, 0 deg C, 2.) 24 h, r.t.
View Scheme
参考文献
Munegumi, Toratane; Meng, Yan-Quing; Harada, Kaoru
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 8 p. 2748 - 2750
反应条件
1: toluene / anfangs unter Kuehlung
2: diethyl ether; MgO / anfangs unter Kuehlung
3: acetic acid anhydride
View Scheme
参考文献
Bergmann; Zervas
Chemische Berichte, 1932 , vol. 65, p. 1192,1198
反应条件
1: chloroform / anfangs unter Kuehlung
2: aqueous NaOH
3: palladium; methanol.acetic acid
View Scheme
参考文献
Grassmann; Schneider
Biochemische Zeitschrift, 1934 , vol. 273, p. 455,460
