5,5-二甲基-1,3-环戊二烯合成路线 (共 17 条)
反应条件
lithium aluminium tetrahydride in diethylene glycol dimethyl ether
1) r.t., 1 h, 2) 80 deg C, 1 h; Yield given. Yields of byproduct given;
参考文献
Roth, Wolfgang R.; Klaerner, Frank-Gerrit; Lennartz, Hans-Werner
Chemische Berichte, 1980 , vol. 113, # 5 p. 1818 - 1829
反应条件
T=24.6 - 54.7°C; isotope effects; KineticsRate constant;
参考文献
Baldwin, John E.; Ghatlia, Naresh D.
Journal of the American Chemical Society, 1989 , vol. 111, # 9 p. 3319 - 3325
参考文献
Mironov,V.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1973 , vol. 22, p. 346 - 352
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1973 , vol. 22, p. 363 - 370
参考文献
McLean,S.; Haynes,P.
Tetrahedron, 1965 , vol. 21, p. 2313 - 2327
反应条件
hydrogen; Pt-Au film
T=181.9 - 383.9°C; effect of temperature and Pt content of Pt-Au films; Rate constantProduct distributionMechanism;
参考文献
Kane, Alan F.; Clarke, John K. A.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1980 , vol. 76, p. 1640 - 1651
反应条件
hydrogen; platinum(IV) oxide in acetic acid
P=2280 Torr;
参考文献
Rouse,S.; Tyler,W.E.
Journal of Organic Chemistry, 1961 , vol. 26, p. 3525 - 3527
反应条件
in dimethyl-ether
T=-40°C; 5 h; Irradiation;
参考文献
Roth, Wolfgang R.; Klaerner, Frank-Gerrit; Lennartz, Hans-Werner
Chemische Berichte, 1980 , vol. 113, # 5 p. 1818 - 1829