反应条件
1.1: N,N-dimethyl-aniline / 6 h / 195 - 200 °C / |Inert atmosphere
2.1: potassium carbonate / acetone / 2 h / |Reflux
3.1: osmium(VIII) oxide; sodium periodate; sodium hydrogencarbonate / methanol; water; toluene / 0.33 h / 20 °C
4.1: methanol; water; toluene / 2 h
5.1: palladium on activated charcoal; hydrogen / methanol / 10 h
6.1: sulfuric acid / 0.25 h / 85 - 90 °C
6.2: 2 h / |Reflux
View Scheme
参考文献
Lahiri, Saswata; Ramarao; Rao, B. Venkateswara; Rao, A.V. Rama; Chorghade, Mukund S.
Organic Process Research and Development, 1999 , vol. 3, # 1 p. 71 - 72
