4-氯甲基-7-甲基色烯-2-酮合成路线 （共 6 条）
反应条件
sulfuric acid in water
T=20°C; Pechmann condensation; 17 h;
参考文献
Fonseca, Andrea S. C.; Goncalves, M. Sameiro T.; Costa, Susana P G.
Amino Acids, 2010 , vol. 39, # 3 p. 699 - 712
反应条件
phosphorus pentachloride in benzene
4 h; Heating;
参考文献
Joshi, S. D.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 399 - 402
反应条件
1: 80 percent / SeO2 / xylene / 12 h / Heating
2: 0.4 g / NaBH4 / methanol / 0.5 h / T < 40 deg C
3: 0.45 g / PCl5 / benzene / 4 h / Heating
View Scheme
参考文献
Joshi, S. D.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 399 - 402
反应条件
1: 0.4 g / NaBH4 / methanol / 0.5 h / T < 40 deg C
2: 0.45 g / PCl5 / benzene / 4 h / Heating
View Scheme
参考文献
Joshi, S. D.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 399 - 402
反应条件
chlorine; acetic acid
参考文献
Dey; Radhabai
Journal of the Indian Chemical Society, 1934 , vol. 11, p. 635,648
反应条件
acetic anhydride
3 h; Heating;
参考文献
Joshi, S. D.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 399 - 402
