4-氯甲基-7-甲氧基色烯-2-酮合成路线 （共 14 条）
反应条件
sodium hydroxide in water T=80°C; 16 h;
参考文献
Piloto, Ana M.; Fonseca, Andrea S.C.; Costa, Susana P.G.; Goncalves, M. Sameiro T.
Tetrahedron, 2006 , vol. 62, # 39 p. 9258 - 9267
反应条件
silica gel supported zirconyl chloride octahydrate
T=90°C; Pechmann condensation reaction; 0.5 h;
参考文献
Karami, Bahador; Kiani, Mahtab
Catalysis Communications, 2011 , vol. 14, # 1 p. 62 - 67
反应条件
potassium carbonate in acetone
T=20°C;
参考文献
Lin, Weiying; Long, Lingliang; Tan, Wen; Chen, Bingbing; Yuan, Lin
Chemistry - A European Journal, 2010 , vol. 16, # 13 p. 3914 - 3917
参考文献
Molecular Probes, Inc.
Patent: US5362628 A1, 1994 ;
参考文献
Molecular Probes, Inc.
Patent: US5576424 A1, 1996 ;
反应条件
1: H2O2; H2SO4 / methanol / 48 h / 20 °C
2: H2SO4 / 2 h / 0 °C
View Scheme
参考文献
Nam, Nguyen-Hai; Kim, Yong; You, Young-Jae; Hong, Dong-Ho; Kim, Hwan-Mook; Ahn, Byung-Zun
Bioorganic and medicinal chemistry letters, 2002 , vol. 12, # 17 p. 2345 - 2348
反应条件
phosphorus pentachloride in benzene
4 h; Heating;
参考文献
Joshi, S. D.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 399 - 402
反应条件
1: 85 percent / SeO2 / xylene / 12 h / Heating
2: 0.32 g / NaBH4 / methanol / 0.5 h / T < 40 deg C
3: 0.4 g / PCl5 / benzene / 4 h / Heating
View Scheme
参考文献
Joshi, S. D.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 399 - 402
反应条件
1: 0.32 g / NaBH4 / methanol / 0.5 h / T < 40 deg C
2: 0.4 g / PCl5 / benzene / 4 h / Heating
View Scheme
参考文献
Joshi, S. D.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 399 - 402
参考文献
Struebe, Frank; Rath, Susann; Mattay, Jochen
European Journal of Organic Chemistry, 2011 , # 24 p. 4645 - 4653
