3,3'-硫代二丙酸二甲酯合成路线 （共 23 条）
反应条件
sodium hydrogensulfide; sodium hydrogencarbonate in methanol; water 1 h; Ambient temperature;
参考文献
Rule; Detty; Kaeding; Sinicropi
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1665 - 1673
反应条件
sodium methylate in methanol
参考文献
Lilly S.A.; Lilly Industries Limited
Patent: US5015656 A1, 1991 ;
反应条件
piperidine T=80°C; 0.166667 h;
参考文献
Dowd, Paul; Choi, Soo-Chang
Tetrahedron, 1991 , vol. 47, # 27 p. 4847 - 4860
反应条件
(NH4)2S; hydrogen sulfide; sulfur in water T=16 - 20°C; Industry scale; Product distribution / selectivity;
参考文献
Beijing Tianqing Chemicals Co., Ltd.
Patent: EP2216331 A1, 2010 ;
Location in patent: Page/Page column 13 ;
反应条件
sulfuric acid Heating;
参考文献
Kumar, Anil; Tilak, B. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 880 - 882
反应条件
in water T=35°C; Michael addition reaction; 0.5 h; Inert atmosphere;
参考文献
Lohier, Jean-Francois; Foucoin, Florian; Jaffres, Paul-Alain; Garcia, Jose I.; Santos, Jana Sopkova-De Oliveira; Perrio, Stephane; Metznert, Patrick
Organic Letters, 2008 , vol. 10, # 6 p. 1271 - 1274
反应条件
sodium sulfide in dimethyl sulfoxide
参考文献
de Jonge,C.R.H.I. et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1973 , p. 1276 - 1279
反应条件
a) 20 deg C, 1 h, b) reflux, 2 h;
参考文献
Vasil'eva, T. P.; Mozzhukhin, A. O.; Antipin, M. Yu.; Struchkov, Yu. T.
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), 1992 , vol. 41, # 8.1 p. 1766 - 1775,1368 - 1376
反应条件
hydrogen sulfide; sodium acetate
参考文献
Volynskii,N.P.; Urin,A.B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 2383 - 2386
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 2504 - 2509
反应条件
sodium methylate in tetrahydrofuran; methanol T=20°C; Dieckmann cyclization; 3 h;
参考文献
Ward, Dale E.; Rasheed, M. Abdul; Gillis, H. Martin; Beye, Garrison E.; Jheengut, Vishal; Achonduh, George T.
Synthesis, 2007 , # 10 p. 1584 - 1586
