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乙二醇
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63148-62-9
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
41317-87-7
合成路线
（共 18 条）
3375-38-0
1,4-二苯甲酰丁烷
→
反应条件
41317-87-7
反应条件
titanium nanoparticles in tetrahydrofuran T=66°C; 6 h; Inert atmosphere;
参考文献
Nador, Fabiana; Mascaro, Evangelina; Castro, Melisa; Vitale, Cristian; Radivoy, Gabriel
Arkivoc, 2011 , vol. 2011, # 7 p. 312 - 326
3375-38-0
1,4-二苯甲酰丁烷
→
反应条件
41317-87-7
+
72930-73-5
反应条件
titanium(IV) isopropylate; titanium; chloro-trimethyl-silane in ethylene glycol dimethyl ether 12 h; Heating;
参考文献
Fuerstner, Alois; Hupperts, Achim
Journal of the American Chemical Society, 1995 , vol. 117, # 16 p. 4468 - 4475
849943-95-9
+
100-59-4
苯基氯化镁
→
反应条件
41317-87-7
反应条件
1: phenyl-magnesium chloride With C24H52Cl2O12P4Pd2 in tetrahydrofuran; 1,4-dioxane T=20°C; Kumada-Corriu cross-coupling reaction; 0.0833333 h; Inert atmosphere; 2: 3,4,5,6-tetrahydro-[1,1'-biphenyl]-2-yl 4-methylbenzenesulfonate in tetrahydrofuran; 1,4-dioxane T=80°C; Kumada-Corriu cross-coupling reaction; 24 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Kapdi, Anant R.; Fenner, Sabine; Kornhaab, Christoph; Schulzke, Carola
Chemistry - A European Journal, 2011 , vol. 17, # 10 p. 2965 - 2971
849943-95-9
+
98-80-6
苯硼酸
→
反应条件
41317-87-7
反应条件
potassium phosphate; CM-phos; palladium diacetate; triethylamine in tert-butyl alcohol T=50°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Wong, Pui Yu; Chow, Wing Kin; Chung, Kin Ho; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemical Communications, 2011 , vol. 47, # 29 p. 8328 - 8330
3375-38-0
1,4-二苯甲酰丁烷
→
反应条件
41317-87-7
+
65926-98-9
反应条件
titanium(III) chloride; zinc in ethylene glycol dimethyl ether 3.5 h; Heating;
参考文献
Fuerstner, Alois; Hupperts, Achim; Ptock, Arne; Janssen, Edo
Journal of Organic Chemistry, 1994 , vol. 59, # 18 p. 5215 - 5229
140903-04-4
→
反应条件
41317-87-7
反应条件
1: yellow mercuric oxide, Na2SO4, sat. KOH-EtOH / diethyl ether / 6 h / Ambient temperature 2: 96 percent Chromat. / 9,10-dicyanoanthracene (DCA) / acetonitrile / 0.08 h / Irradiation; also with Cu(II)-perchlorate View Scheme
参考文献
Ishiguro, Katsuya; Ikeda, Masatoshi; Sawaki, Yasuhiko
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3057 - 3066
21266-01-3
→
反应条件
41317-87-7
反应条件
Cu(II) perchlorate in acetonitrile Ambient temperature;
参考文献
Ishiguro, Katsuya; Sawaki, Yasuhiko; Iwamura, Hiizu
Chemistry Letters, 1987 , p. 1853 - 1856
591-50-4
碘苯
+
110-83-8
环己烯
→
反应条件
92-52-4
联苯
+
771-98-2
1-苯基-1-环己烯
+
4994-16-5
+
10470-07-2
+
109245-21-8
+
41317-87-7
+
93874-12-5
+
10468-71-0
反应条件
palladium diacetate; potassium hydroxide T=140°C; Heck reaction; 4 h; Inert atmosphereIonic liquid; regioselective reaction;
参考文献
Mieczynska, Ewa; Trzeciak, Anna M.
Molecules, 2010 , vol. 15, # 4 p. 2166 - 2177
591-50-4
碘苯
+
110-83-8
环己烯
→
反应条件
771-98-2
1-苯基-1-环己烯
+
4994-16-5
+
10470-07-2
+
109245-21-8
+
41317-87-7
+
93874-12-5
+
10468-71-0
反应条件
Pd/Al2O3 + Fe2O3; potassium hydroxide in N,N-dimethyl-formamide T=140°C; Heck reaction; 4 h; Inert atmosphere; regioselective reaction;
参考文献
Mieczynska, Ewa; Trzeciak, Anna M.
Molecules, 2010 , vol. 15, # 4 p. 2166 - 2177
1072-21-5
己二醛
→
反应条件
41317-87-7
反应条件
1.1: iodine; magnesium / diethyl ether / Inert atmosphere; Reflux 1.2: 0 °C / Inert atmosphere 2.1: PDC / dichloromethane / 20 °C 3.1: titanium nanoparticles / tetrahydrofuran / 6 h / 66 °C / Inert atmosphere View Scheme
参考文献
Nador, Fabiana; Mascaro, Evangelina; Castro, Melisa; Vitale, Cristian; Radivoy, Gabriel
Arkivoc, 2011 , vol. 2011, # 7 p. 312 - 326
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