反应条件
in diethyl ether
1 mol of complex was slowly added to an ether soln. of 2 mol RMgCl at -15°C, after 1 h the temp. was raised to 0°C (Ar atm.);; dioxane in hexane was added, ppt. was filtered off, identified by ESR spectra;;
参考文献
Razuvaev, G.A.; Latyaeva, V.N.; Vyshinskaya, L.I.; Drobotenko, V.V.
Journal of Organometallic Chemistry, 1981 , vol. 208, # 2 p. 169 - 182
