2,4-二甲氧基-4-羟基二苯甲酮合成路线 （共 7 条）
反应条件
zinc(II) chloride; trichlorophosphate T=60 - 70°C; 2 h;
参考文献
Vinaya, Kambappa; Kavitha, Chandagirikoppal V.; Prasanna, Doddakunche S.; Chandrappa, Siddappa; Ranganatha, Somasagara R.; Raghavan, Sathees C.; Rangappa, Kanchugarakoppal S.
Chemical Biology and Drug Design, 2012 , vol. 79, # 3 p. 360 - 367
反应条件
1: 88 percent / K2CO3, KI / ethanol / 72 h / Heating 2: 91 percent / 2 N NaOH / ethanol / 16 h / Heating 3: 85 percent / NH2OH*HCl, triethylamine / methanol; H2O / 72 h / Heating 4: 98 percent / hydrogen / PtO2 / acetic acid / 336 h / 760 Torr View Scheme
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 56, # 9 p. 1506 - 1507
反应条件
1: 88 percent / K2CO3, KI / ethanol / 72 h / Heating 2: 91 percent / 2 N NaOH / ethanol / 16 h / Heating 3: 85 percent / NH2OH*HCl, triethylamine / methanol; H2O / 72 h / Heating 4: 98 percent / hydrogen / PtO2 / acetic acid / 336 h / 760 Torr 5: 84 percent / K2CO3 / dioxane; H2O / 3 h View Scheme
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 56, # 9 p. 1506 - 1507
反应条件
1: 88 percent / K2CO3, KI / ethanol / 72 h / Heating 2: 91 percent / 2 N NaOH / ethanol / 16 h / Heating 3: 85 percent / NH2OH*HCl, triethylamine / methanol; H2O / 72 h / Heating 4: 98 percent / hydrogen / PtO2 / acetic acid / 336 h / 760 Torr 5: 84 percent / K2CO3 / dioxane; H2O / 3 h View Scheme
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 56, # 9 p. 1506 - 1507
参考文献
Ciba-Geigy Corporation
Patent: US4859736 A1, 1989 ;
反应条件
potassium carbonate
10 h; Reflux;
参考文献
Vinaya, Kambappa; Kavitha, Chandagirikoppal V.; Prasanna, Doddakunche S.; Chandrappa, Siddappa; Ranganatha, Somasagara R.; Raghavan, Sathees C.; Rangappa, Kanchugarakoppal S.
Chemical Biology and Drug Design, 2012 , vol. 79, # 3 p. 360 - 367
反应条件
1: 88 percent / K2CO3, KI / ethanol / 72 h / Heating
2: 91 percent / 2 N NaOH / ethanol / 16 h / Heating
View Scheme
参考文献
Sawada, Seiji; Yasui, Kumiko; Takahashi, Sho
Bioscience, Biotechnology, and Biochemistry, 1992 , vol. 56, # 9 p. 1506 - 1507
