2-羟基-1-(4-甲氧基苯基)-1-乙酮合成路线 （共 46 条）
反应条件
in acetone T=25°C; 3 h;
参考文献
Kovac, F.; Baumstark, A. L.
Tetrahedron Letters, 1994 , vol. 35, # 47 p. 8751 - 8754
反应条件
oxygen in chlorobenzene T=95°C; P=757.6 Torr; var. of temp., further addition of cumene, ΔEa; Product distributionKineticsThermodynamic data;
参考文献
Suprun, Wladimir
Advanced Synthesis and Catalysis, 1996 , vol. 338, # 3 p. 231 - 237
反应条件
1.1: m-CPBA / H2O / 2 h / 20 °C 1.2: 15 percent / sulfuric acid / H2O / 2 h 2.1: 95 percent / 4-dimethylaminopyridine; triethylamine / CH2Cl2 / 20 °C 3.1: tetrapropylammonium perruthenate; N-methylmorpholine N-oxide / CH2Cl2 / 3 h / 20 °C 3.2: 386 mg / Oxone / H2O; methanol / 3 h / 20 °C View Scheme
参考文献
Tsujigami, Toshikuni; Sugai, Takeshi; Ohta, Hiromichi
Tetrahedron Asymmetry, 2001 , vol. 12, # 18 p. 2543 - 2549
反应条件
1: 86 percent / 4-methylmorpholine 4-oxide dihydrate, osmium tetroxide / acetone; 2-methyl-propan-2-ol / 48 h / Ambient temperature 2: 76 percent / NaHCO3 / H2O; methanol / 1.5 h / Heating View Scheme
参考文献
Waszkuc, Wieslaw; Janecki, Tomasz; Bodalski, Ryszard
Synthesis, 1984 , # 12 p. 1025 - 1027
反应条件
1: 85 percent / 50percent aq. NaOH / CH2Cl2 / 25 °C 2: 86 percent / 4-methylmorpholine 4-oxide dihydrate, osmium tetroxide / acetone; 2-methyl-propan-2-ol / 48 h / Ambient temperature 3: 76 percent / NaHCO3 / H2O; methanol / 1.5 h / Heating View Scheme
参考文献
Waszkuc, Wieslaw; Janecki, Tomasz; Bodalski, Ryszard
Synthesis, 1984 , # 12 p. 1025 - 1027
反应条件
air; triethylamine in acetone 5 h; Irradiation;
参考文献
Chai, Wen; Takeda, Akihiro; Hara, Makoto; Ji, Shun-Jun; Horiuchi, C. Akira
Tetrahedron, 2005 , vol. 61, # 9 p. 2453 - 2463
反应条件
1: sodium tetrahydroborate / methanol / 20 °C 2: silica gel; C26H51N2O2(1+)*BF4(1-) / dichloromethane / 1.5 h / 20 °C View Scheme
参考文献
Nguyen, John D.; Matsuura, Bryan S.; Stephenson, Corey R. J.
Journal of the American Chemical Society, 2014 , vol. 136, # 4 p. 1218 - 1221
反应条件
1: sodium chloride / acetonitrile 2: methanol / 25 °C View Scheme
参考文献
Tagawa, Kohei; Sasagawa, Keita; Wakisaka, Ken; Monjiyama, Shunsuke; Katayama, Mika; Yamataka, Hiroshi
Bulletin of the Chemical Society of Japan, 2014 , vol. 87, # 1 p. 119 - 126
反应条件
2,4,6-triphenylpyrylium-tetrafluoroborate 4 h; Irradiation;
参考文献
Memarian, Hamid R.; Nikpour, Farzad
Monatshefte fur Chemie, 2002 , vol. 133, # 7 p. 1045 - 1053
反应条件
2,4,6-triphenylpyrylium-tetrafluoroborate 10 h; Irradiation;
参考文献
Memarian, Hamid R.; Nikpour, Farzad
Monatshefte fur Chemie, 2002 , vol. 133, # 7 p. 1045 - 1053
