2-羟基-1-(4-甲氧基苯基)-1-乙酮合成路线 (共 46 条)
反应条件
ammonium hydroxide; copper diacetate
参考文献
Weidenhagen; Herrmann
Chemische Berichte, 1935 , vol. 68, p. 1953,1956
反应条件
1: potassium tert-butylate / tetrahydrofuran / 0 - 80 °C / |Inert atmosphere 2: sulfuric acid / |Reflux; |Inert atmosphere View Scheme
参考文献
Synthetic Communications, , vol. 43, # 11 p. 1549 - 1556
反应条件
methanol; lead(II) hydroxide on calcium carbonate
参考文献
Krueger
Chemische Berichte, 1956 , vol. 89, p. 1016,1018
反应条件
oxygen; copper dichloride in toluene
T=100°C; 10 h; Molecular sieve;
参考文献
Cho, Chan Sik; Ren, Wen Xiu
Journal of Organometallic Chemistry, 2009 , vol. 694, # 19 p. 3215 - 3217
反应条件
1: potassium carbonate / acetonitrile / 24 h / Reflux
2: iodine; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) / methanol; dichloromethane / 20 h
3: potassium carbonate / acetone / Inert atmosphere; Reflux
4: acetonitrile / Inert atmosphere
5: potassium tert-butylate / methanol / Inert atmosphere; Reflux
6: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1800.18 Torr
View Scheme
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607
反应条件
potassium carbonate in acetonitrile
24 h; Reflux;
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607