3,3-二甲基-2-氧代丁酸钾盐合成路线 (共 2 条)
反应条件
pyridine; 1,10-phenanthroline; tris-(o-tolyl)phosphine; copper(I) bromide in 1-methyl-pyrrolidin-2-one T=170°C; 36 h;
参考文献
SALTIGO GMBH
Patent: US2009/221832 A1, 2009 ;
Location in patent: Page/Page column 2-3 ;
反应条件
copper(I) oxide; 1,10-phenanthroline; tris(4-methylphenyl)-phosphine; PdI2 in 1-methyl-pyrrolidin-2-one T=170°C; 16 h; Inert atmosphere;
参考文献
Goossen, Lukas J.; Linder, Christophe; Rodriguez, Nuria; Lange, Paul P.
Chemistry - A European Journal, 2009 , vol. 15, # 37 p. 9336 - 9349