1,1'-(1,2-乙二基)二[二苯基-氧膦]合成路线 （共 36 条）
反应条件
sodium hydroxide
T=25°C; 0.5 h; Further byproducts given;
参考文献
Jaeger, David A.; Bolikal, Durgadas
Journal of Organic Chemistry, 1986 , vol. 51, # 8 p. 1350 - 1352
反应条件
oxygen
T=80°C; 18 h;
参考文献
Hirai, Takayoshi; Han, Li-Biao
Organic Letters, 2007 , vol. 9, # 1 p. 53 - 55
反应条件
1: 73 percent / dimethylformamide / 10 h / Heating
2: 1.7 percent / aq. NaOH / 10 h / Heating
View Scheme
参考文献
Calcagno, Patrizia; Kariuki, Benson M.; Kitchin, Simon J.; Robinson, James M. A.; Philp, Douglas; Harris, Kenneth D. M.
Chemistry - A European Journal, 2000 , vol. 6, # 13 p. 2338 - 2349
反应条件
in tetrahydrofuran
T=20°C; 5 h;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
in tetrahydrofuran
T=20°C;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
in tetrahydrofuran
T=20°C; 3 h;
参考文献
Boulos, Leila S.; Ewies, Ewies F.; Fahmy, Amin F. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 726 - 738
反应条件
1: 75 percent / NEt3 / tetrahydrofuran / 2.5 h / 0 - 20 °C
2: 9.1 percent / 250 °C
View Scheme
参考文献
Baldwin, Lawrence C; Fink, Mark J
Journal of Organometalic Chemistry, 2002 , vol. 646, # 1-2 p. 230 - 238
反应条件
sodium hydroxide in methanol; water
参考文献
Cristau; Virieux
Tetrahedron Letters, 1999 , vol. 40, # 4 p. 703 - 706
反应条件
sodium hydroxide
Hydrolysis; 10 h; Heating;
参考文献
Calcagno, Patrizia; Kariuki, Benson M.; Kitchin, Simon J.; Robinson, James M. A.; Philp, Douglas; Harris, Kenneth D. M.
Chemistry - A European Journal, 2000 , vol. 6, # 13 p. 2338 - 2349
反应条件
1: 97 percent / KOH / dimethylsulfoxide; H2O / 1 h
2: hydrogen peroxide / H2O
View Scheme
参考文献
Khachatryan, R. A.; Sayadyan, S. V.; Grigoryan, N. Yu.; Indzhikyan, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 11 p. 2472 - 2478,2197 - 2203
