3,5-二羟基苯甲酸乙酯合成路线 (共 27 条)
反应条件
hydrogenchloride 360 h; Heating;
参考文献
Abidi, Rym; Asfari, Zouhair; Harrowfield, Jack M.; Nauman, Christoph; Sobolev, Alexander N.; Vicens, Jacques
Anales de Quimica, 1996 , vol. 92, # 1 p. 51 - 56
反应条件
Candida cylindracea lipase in di-isopropyl ether; butan-1-ol T=28 - 30°C; 3 h;
参考文献
Parmar, Virinder S.; Kumar, Ajay; Bicht, Kirpal S.; Mukherjee, Shubhasish; Prasad, Ashok K.; Sharma, Sunil K.; Wengel, Jesper; Olsen, Carl E.
Tetrahedron, 1997 , vol. 53, # 6 p. 2163 - 2176
反应条件
palladium 10 on activated carbon; hydrogen; potassium carbonate in ethanol; ethyl acetate T=25°C; 2 h;
参考文献
Cheung, Siu-Yin; Chow, Hak-Fun; Ngai, To; Wei, Xiaoling
Chemistry - A European Journal, 2009 , vol. 15, # 10 p. 2278 - 2288
反应条件
sodium hydrogencarbonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=40°C; 0.666667 h;
参考文献
Ambika; Singh, Pradeep Pratap; Chauhan
Synthetic Communications, 2008 , vol. 38, # 6 p. 928 - 936
反应条件
sulfuric acid; acetic acid T=120°C; 3 h; Neat (no solvent); chemoselective reaction;
参考文献
Rekha; Ramani, Modukuri V.; Ratnamala; Rupakalpana, Vempati; Subbaraju, Gottumukkala V.; Satyanarayana, Chava; Rao, C. Someswara
Organic Process Research and Development, 2009 , vol. 13, # 4 p. 769 - 773
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in tetrahydrofuran; water T=85 - 90°C; 48 h;
参考文献
Carter, Rhiannon R.; Wyatt, Justin K.
Tetrahedron Letters, 2006 , vol. 47, # 34 p. 6091 - 6094
反应条件
1: potash / beim Schmelzen 2: HCl View Scheme
参考文献
Barth; Senhofer
Justus Liebigs Annalen der Chemie, 1871 , vol. 159, p. 222,229
Justus Liebigs Annalen der Chemie, 1872 , vol. 164, p. 109
反应条件
ethanol; potassium carbonate T=130°C;
参考文献
Barth; Senhofer
Justus Liebigs Annalen der Chemie, 1872 , vol. 164, p. 118
参考文献
Fritsch
Justus Liebigs Annalen der Chemie, 1897 , vol. 296, p. 357
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Imai, Hiroyasu; Nakagawa, Shigeo; Kyuno, Eishin
Journal of the American Chemical Society, 1992 , vol. 114, # 17 p. 6719 - 6723