3,5-二羟基苯甲酸乙酯合成路线 （共 27 条）
反应条件
1: potash; alcohol / 130 °C 2: KOH-solution View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 164, p. 118
反应条件
potassium carbonate in acetone T=55°C; 3 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 8 p. 1793 - 1798
参考文献
Justus Liebigs Annalen der Chemie, , vol. 296, p. 357
参考文献
Chemische Berichte, , vol. 35, p. 2885 Anm.
反应条件
1: 63 percent / K2CO3/KI / acetone / 24 h / Heating 2: 100 percent / KOH / aq. ethanol / 3 h / Heating View Scheme
参考文献
Zerban, Georg; Meier, Herbert
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1993 , vol. 48, # 2 p. 171 - 184
反应条件
1: 63 percent / K2CO3/KI / acetone / 24 h / Heating 2: 100 percent / KOH / aq. ethanol / 3 h / Heating 3: 100 percent / SOCl2 / 5 h / 90 °C View Scheme
参考文献
Zerban, Georg; Meier, Herbert
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1993 , vol. 48, # 2 p. 171 - 184
反应条件
sodium formate; palladium on activated charcoal in ethanol
T=30 - 40°C; 3 h;
参考文献
NIPPON KAYAKU KABUSHIKI KAISHA
Patent: EP1571148 A1, 2005 ;
Location in patent: Page/Page column 26 ;
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=0 - 20°C;
参考文献
Del Amo, Vicente; Dubbaka, Srinivas Ready; Krasovskiy, Arkady; Knochel, Paul
Angewandte Chemie - International Edition, 2006 , vol. 45, # 46 p. 7838 - 7842
反应条件
iodine; sodium hydrogencarbonate in tetrahydrofuran; water
T=20°C; 140 h;
参考文献
Visitaev, Yulia; Goldberg, Israel; Vigalok, Arkadi
Inorganic Chemistry, 2013 , vol. 52, # 12 p. 6779 - 6781
反应条件
1: K2CO3
2: lithium aluminium hydride
View Scheme
参考文献
Sivanandan, Kulandaivelu; Vutukuri, Dharmarao; Thayumanavan
Organic Letters, 2002 , vol. 4, # 21 p. 3751 - 3753
