5-(3-氯苯基)-1H-四唑合成路线 （共 9 条）
反应条件
1: With sodium azide in N,N-dimethyl-formamide T=120°C; 36 h; 2: With hydrogenchloride in water; ethyl acetate 0.0833333 h;
参考文献
Lang, Leiming; Li, Baojun; Liu, Wei; Jiang, Li; Xu, Zheng; Yin, Gui
Chemical Communications, 2010 , vol. 46, # 3 p. 448 - 450
反应条件
1: CuO / N,N-dimethyl-formamide / 100 °C 2: CuO; sodium azide / N,N-dimethyl-formamide View Scheme
参考文献
Yapuri, Umanadh; Palle, Sadanandam; Gudaparthi, Omprakash; Narahari, Srinivasa Reddy; Rawat, Dhwajbahadur K.; Mukkanti, Khagga; Vantikommu, Jyothi
Tetrahedron Letters, 2013 , vol. 54, # 35 p. 4732 - 4734
反应条件
1: Na2S2O5; POCl3 2: acetic acid; butan-1-ol; NaN3 View Scheme
参考文献
Herbst; Wilson
Journal of Organic Chemistry, 1957 , vol. 22, p. 1142,1145
参考文献
Koldobskii, G. I.; Ivanova, S. E.
Russian Journal of General Chemistry, 1994 , vol. 64, # 10.2 p. 1512 - 1517
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 10 p. 1698 - 1704
反应条件
in 1,3,5-trimethyl-benzene
T=160 - 170°C; 1 h;
参考文献
Uher, Michal; Foltin, Jozef; Povazanec, Frantisek; Kovac, Jaroslav
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 6 p. 1492 - 1494
反应条件
sodium hydroxide; tetrabutylammomium bromide
1) CH2Cl2, 25 deg C, 3 h, 2) 80 - 130 deg C; Yield given. Multistep reaction;
参考文献
Osipova, T. P.; Koldobskii, G. I.; Ostrovskii, V. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 5 p. 1018 - 1019
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 1119 - 1120
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane
T=25°C; 5 h; Product distribution;
参考文献
Osipova, T. F.; Ostrovskii, V. A.; Koldobskii, G. I.; Erusalimskii, G. B.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 357 - 362
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 398 - 404
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane
T=25°C; 5 h; Product distribution;
参考文献
Osipova, T. F.; Ostrovskii, V. A.; Koldobskii, G. I.; Erusalimskii, G. B.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 357 - 362
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 398 - 404
参考文献
Koldobskii, G. I.; Ivanova, S. E.
Russian Journal of General Chemistry, 1994 , vol. 64, # 10.2 p. 1512 - 1517
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 10 p. 1698 - 1704
