SO2Cl2 in dichloromethane
byproducts: SO2; under N2, to Me2SbSbMe2 in CH2Cl2 at -78°C was added SO2Cl2 (molar ratio) in CH2Cl2, mixt. was srirred; CH2Cl2 and SO2 were evapd.;
参考文献
Stevens, J. G.; Trooster, J. M.; Meinema, H. A.; Noltes, J. G.
Inorganic Chemistry, 1981 , vol. 20, p. 801 - 803
in neat (no solvent)
inert atmosphere; dropwise addn. of 1 equiv. Me4Sb2 to Et2Te2 at 0°C, standing for 1 d; filtration, vac. distn. off of volatiles (bath at 25-30°C); contg. 4percent Et2Te2 as impurity;
参考文献
Dickson, Ron S.; Heazle, Kerryn D.
Journal of Organometallic Chemistry, 1995 , vol. 493, # 1-2 p. 189 - 198
