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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4--甲氧基黄酮
合成路线
（共 114 条）
3327-24-0
2'-羟基-2-(4-甲氧基亚苄基)乙酰苯
→
反应条件
4143-74-2
4--甲氧基黄酮
反应条件
iodine in dimethyl sulfoxide 1 h; Reflux;
参考文献
Sagrera, Gabriel; Seoane, Gustavo
Synthesis, 2010 , # 16 art. no. M06509SS, p. 2776 - 2786
101278-20-0
→
反应条件
4143-74-2
4--甲氧基黄酮
反应条件
4-(N,N-dimethlyamino)pyridine in N,N-dimethyl-formamide T=0 - 30°C; Morita-Baylis-Hillman reaction; 2 h; Inert atmosphere; regioselective reaction;
参考文献
Yoshida, Masahito; Fujino, Yuta; Saito, Koya; Doi, Takayuki
Tetrahedron, 2011 , vol. 67, # 51 p. 9993 - 9997
3034-08-0
4-甲氧基黄烷酮
→
反应条件
4143-74-2
4--甲氧基黄酮
反应条件
Tl(Oac)3 in acetic acid 3 h; Heating;
参考文献
Khanna, Mahavir S.; Singh, Om V.; Garg, Chandra P.; Kapoor, Ram P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 19 p. 2565 - 2568
201230-82-2
+
95-56-7
邻溴苯酚
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
4143-74-2
4--甲氧基黄酮
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1-methyl-2-((4-phenyl-1H-1,2,3-triazol-1-yl)methyl)-1H-benzo[d]imidazole; n-dipropylamine T=130°C; P=15001.5 Torr; 24 h; Autoclave;
参考文献
Liu, Jianming; Liu, Muwen; Yue, Yuanyuan; Zhang, Ningfei; Zhang, Yuanli; Zhuo, Kelei
Tetrahedron Letters, 2013 , vol. 54, # 14 p. 1802 - 1807
118-93-4
2'-羟基苯乙酮
+
100-07-2
对甲氧基苯甲酰氯
→
反应条件
4143-74-2
4--甲氧基黄酮
反应条件
1: With potassium tert-butylate in tetrahydrofuran T=0 - 67°C; 2: With sulfuric acid in acetic acid 2.5 h; Heating; Further stages.;
参考文献
McKendall, Michael; Smith, Tasha; Anh, Kien; Ellis, Jamie; McGee, Terri; Foroozesh, Maryam; Zhu, Naijue; Stevens, Cheryl L. Klein
Journal of Chemical Crystallography, 2008 , vol. 38, # 4 p. 231 - 237
4143-72-0
1-(1-羟基苯基)-3-(4-甲氧基苯基)丙烷-1,3-二酮
→
反应条件
4143-74-2
4--甲氧基黄酮
反应条件
gallium trifluoromethanesulfonate in nitromethane T=80°C; 2 h;
参考文献
Su; Zhu; Li
Organic Preparations and Procedures International, 2009 , vol. 41, # 1 p. 69 - 75
58721-41-8
→
反应条件
4143-74-2
4--甲氧基黄酮
反应条件
iodine T=100 - 110°C; 1.4 h; Neat (no solvent);
参考文献
Sashidhara, Koneni V.; Kumar, Manoj; Kumar, Abdhesh
Tetrahedron Letters, 2012 , vol. 53, # 18 p. 2355 - 2359
533-58-4
2-碘苯酚
+
201230-82-2
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
36685-41-3
+
4143-74-2
4--甲氧基黄酮
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; Pd(OAc)2(dppf)2 in N,N-dimethyl-formamide T=60°C; P=760 Torr; 6 h;
参考文献
Ciattini, Pier Giuseppe; Morera, Enrico; Ortar, Giorgio; Rossi, Sabina Strano
Tetrahedron, 1991 , vol. 47, # 32 p. 6449 - 6456
34000-29-8
→
反应条件
4143-74-2
4--甲氧基黄酮
反应条件
selenium(IV) oxide; silica gel in dimethyl sulfoxide Cyclization; 0.1 h; Microwave irradiation;
参考文献
Gupta, Mukta; Paul, Satya; Gupta, Rajive; Loupy, Andre
Organic Preparations and Procedures International, 2000 , vol. 32, # 3 p. 280 - 283
533-58-4
2-碘苯酚
+
201230-82-2
+
3989-14-8
(4-甲氧基苯乙炔基)三甲基硅烷
→
反应条件
4143-74-2
4--甲氧基黄酮
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tetrabutyl ammonium fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; (Me)CgPPh in tetrahydrofuran; N,N-dimethyl-formamide T=90°C; microwave-assisted Sonogashira-carbonylation-cyclization reaction; P=760.051 Torr; 0.5 h; Microwave irradiation;
参考文献
Awuah, Emelia; Capretta, Alfredo
Organic Letters, 2009 , vol. 11, # 15 p. 3210 - 3213
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