2-甲基-4-羟基苯甲醛合成路线 （共 26 条）
反应条件
formic acid; triphenylphosphine; palladium diacetate in ethyl acetate
参考文献
Eli Lilly and Company
Patent: US6156748 A1, 2000 ;
反应条件
sodium hydroxide in water T=60°C; 8 h;
参考文献
Hodgson; Jenkinson
Journal of the Chemical Society, 1929 , p. 469,470
反应条件
hydrogenchloride in tetrahydrofuran; methanol; water T=50°C; 1.5 h;
参考文献
Kissei Pharmaceutical Co., Ltd.
Patent: EP1544208 A1, 2005 ;
Location in patent: Page/Page column 59-60 ;
反应条件
boron trifluoride diethyl etherate; water; mercury(II) oxide in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Jo, Shigeo; Tanimoto, Shigeo; Sugimoto, Toyonari; Okano, Masaya
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 7 p. 2120 - 2123
反应条件
pseudomonas-cultures; water T=30°C; bei pH 7;
参考文献
Dagley; Patel
Biochemical Journal, 1957 , vol. 66, p. 227,231
反应条件
pyridine hydrochloride T=180 - 190°C; Yield given;
参考文献
Charlton, James L.; Koh, Kevin
Tetrahedron Letters, 1988 , vol. 29, # 44 p. 5595 - 5598
反应条件
1: Br2 / CCl4 2: 1.) Mg / 1.) THF 3: Py.HCl / 180 - 190 °C View Scheme
参考文献
Charlton, James L.; Koh, Kevin
Tetrahedron Letters, 1988 , vol. 29, # 44 p. 5595 - 5598
反应条件
1: BF3*Et2O / CH2Cl2 / 14 h / Ambient temperature 2: 91 percent / H2O, HgO, BF3*Et2O / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Love
J. roy. tech. Coll., 1935 , vol. 3, p. 385
反应条件
hydrogenchloride; aluminium trichloride in benzene
参考文献
Laarhoven,W.H. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1961 , vol. 80, p. 775 - 791
反应条件
titanium tetrachloride
参考文献
Nakamura, Yosuke; O-kawa, Kyoji; Minami, Satoshi; Ogawa, Toshio; Tobita, Seiji; Nishimura, Jun
Journal of Organic Chemistry, 2002 , vol. 67, # 4 p. 1247 - 1252
