in dichloromethane byproducts: C6H5NH2; under N2, to CH2Cl2 simultaneously added dropwise MeBBr2 (0.1 mole) and0.1 mole of mixt. of O(SiMe3)2 (0.066 mole) and PhN(SiMe3)2 (0.033 mole) at room temp., refluxed for 6 h; evapd., sepd. by distn.;
参考文献
Oesterle, Rainer; Maringgele, Walter; Meller, Anton
Journal of Organometallic Chemistry, 1985 , vol. 284, p. 281 - 290
Lee, Soon W.; Miller, Glenn A.; Campana, Charles F.; Maciejewski, Mary L.; Trogler, William C.
Journal of the American Chemical Society, 1987 , vol. 109, # 16 p. 5050 - 5051
Lee, Soon W.; Miller, Glenn A.; Campana, Charles F.; Maciejewski, Mary L.; Trogler, William C.
Journal of the American Chemical Society, 1987 , vol. 109, # 16 p. 5050 - 5051
Lee, Soon W.; Miller, Glenn A.; Campana, Charles F.; Maciejewski, Mary L.; Trogler, William C.
Journal of the American Chemical Society, 1987 , vol. 109, # 16 p. 5050 - 5051