2-[(乙氧羰基)氨基]苯甲酸合成路线 （共 27 条）
反应条件
lithium hydroxide in tetrahydrofuran; water
T=20°C;
参考文献
Correa, Arkaitz; Tellitu, Imanol; Dominguez, Esther; SanMartin, Raul
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3501 - 3505
反应条件
potassium hydroxide in ethanol; water; benzene
Heating;
参考文献
Martin, Dieter; Nadolski, Karin; Gruendemann, Egon
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 5 p. 737 - 746
反应条件
1: C8H7O3(1-)*Li(1+); benzoic acid lithium salt With palladium diacetate in 1,4-dioxane
T=100°C; 0.5 h; Inert atmosphereSealed tube;
2: ethyl N-mesitylsulfonyloxycarbamate in 1,4-dioxane
T=100°C; 0.5 h; Inert atmosphereSealed tube;
3: With hydrogenchloride in 1,4-dioxane; water; ethyl acetate
T=20°C; Inert atmosphere;
参考文献
Ng, Ka-Ho; Ng, Fo-Ning; Yu, Wing-Yiu
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 95 p. 11680 - 11682,3
反应条件
1: benzoic acid lithium salt; lithium 3-chlorobenzoate With palladium diacetate in 1,4-dioxane
T=100°C; 0.5 h; Inert atmosphereSealed tube;
2: ethyl N-mesitylsulfonyloxycarbamate in 1,4-dioxane
T=100°C; 0.5 h; Inert atmosphereSealed tube;
3: With hydrogenchloride in 1,4-dioxane; water; ethyl acetate
T=20°C; Inert atmosphere;
参考文献
Ng, Ka-Ho; Ng, Fo-Ning; Yu, Wing-Yiu
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 95 p. 11680 - 11682,3
反应条件
1: benzoic acid lithium salt; lithium 3-fluorobenzoate With palladium diacetate in 1,4-dioxane
T=100°C; 0.5 h; Inert atmosphereSealed tube;
2: ethyl N-mesitylsulfonyloxycarbamate in 1,4-dioxane
T=100°C; 0.5 h; Inert atmosphereSealed tube;
3: With hydrogenchloride in 1,4-dioxane; water; ethyl acetate
T=20°C; Inert atmosphere;
参考文献
Ng, Ka-Ho; Ng, Fo-Ning; Yu, Wing-Yiu
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 95 p. 11680 - 11682,3
反应条件
1: benzoic acid lithium salt; lithium 3-bromobenzoate With palladium diacetate in 1,4-dioxane
T=100°C; 0.5 h; Inert atmosphereSealed tube;
2: ethyl N-mesitylsulfonyloxycarbamate in 1,4-dioxane
T=100°C; 0.5 h; Inert atmosphereSealed tube;
3: With hydrogenchloride in 1,4-dioxane; water; ethyl acetate
T=20°C; Inert atmosphere;
参考文献
Ng, Ka-Ho; Ng, Fo-Ning; Yu, Wing-Yiu
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 95 p. 11680 - 11682,3
反应条件
1: ClSO2NH2
2: (i) nBu3N, (ii) /BRN= 385653/, (iii) aq. NH3
View Scheme
参考文献
Cohen,E.; Klarberg,B.
Journal of the American Chemical Society, 1962 , vol. 84, p. 1994 - 2002
反应条件
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C
2: lithium hydroxide hydrate; water / methanol / 12 h
View Scheme
参考文献
Vijayadas, Kuruppanthara N.; Nair, Roshna V.; Gawade, Rupesh L.; Kotmale, Amol S.; Prabhakaran, Panchami; Gonnade, Rajesh G.; Puranik, Vedavadi G.; Rajamohanan, Pattuparambil R.; Sanjayan, Gangadhar J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 48 p. 8348 - 8356
反应条件
1: 37 percent / triethylamine / 3 h / Ambient temperature
2: 88 percent / KOH / benzene; ethanol; H2O / Heating
View Scheme
参考文献
Martin, Dieter; Nadolski, Karin; Gruendemann, Egon
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 5 p. 737 - 746
反应条件
(i) nBu3N, (ii) /BRN= 385653/, (iii) aq. NH3; Multistep reaction;
参考文献
Cohen,E.; Klarberg,B.
Journal of the American Chemical Society, 1962 , vol. 84, p. 1994 - 2002
