diethylamine; trichlorophosphate in hexane
3 h; Heating;
参考文献
Connolly, David J.; Lacey, Patrick M.; McCarthy, Mary; Saunders, Cormac P.; Carroll, Anne-Marie; Goddard, Richard; Guiry, Patrick J.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6572 - 6589
Connolly, David J.; Lacey, Patrick M.; McCarthy, Mary; Saunders, Cormac P.; Carroll, Anne-Marie; Goddard, Richard; Guiry, Patrick J.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6572 - 6589
1.1: 97 percent / HCl / hexane / 4.5 h / 0 - 5 °C
2.1: Na; MeOH / cooling
2.2: 65 percent / methanol / 6.5 h / 25 - 80 °C
3.1: 88 percent / N,N-diethylaniline; POCl3 / benzene / 3 h / Heating
View Scheme
参考文献
Connolly, David J.; Lacey, Patrick M.; McCarthy, Mary; Saunders, Cormac P.; Carroll, Anne-Marie; Goddard, Richard; Guiry, Patrick J.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6572 - 6589
Connolly, David J.; Lacey, Patrick M.; McCarthy, Mary; Saunders, Cormac P.; Carroll, Anne-Marie; Goddard, Richard; Guiry, Patrick J.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6572 - 6589