1: Triton-B / methanol / 10 h / Heating
2: 20 g / conc. HCl / 20 h / 120 °C
3: 54 percent / conc. H2SO4 / 24 h / Ambient temperature
View Scheme
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Lal, B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 3 p. 300 - 302
1: Triton-B / methanol / Heating
2: conc. HCl / 120 °C
3: 90 percent / conc. H2SO4 / 24 h / Ambient temperature
4: 90 percent / conc. H2SO4 / 10 h / Heating
View Scheme
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Lal, B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 3 p. 300 - 302
1: PhCH2MgX With copper(l) iodide in tetrahydrofuran
T=20°C;
2: dimethyl glutaconate With chloro-trimethyl-silane in tetrahydrofuran
T=-78 - 20°C; Michael addition;
参考文献
Chang, Chih-Shiang; Lin, Ying-Ting; Shih, Shin-Ru; Lee, Chung-Chi; Lee, Yen-Chun; Tai, Chia-Liang; Tseng, Sung-Nien; Chern, Jyh-Haur
Journal of Medicinal Chemistry, 2005 , vol. 48, # 10 p. 3522 - 3535
