环戊-2-烯-1,4-二醇合成路线 (共 5 条)
反应条件
1: CrO3, aq. H2SO4 / CH2Cl2 / 1 h / -5 °C 2: H2 / Raney Nickel / methanol View Scheme
参考文献
Reimann; Poschl
Pharmazie, 1995 , vol. 50, # 9 p. 589 - 592
反应条件
pyridine; toluene-4-sulfonic acid in tetrahydrofuran; diethyl ether; dichloromethane
参考文献
Kowa Company, Ltd.
Patent: US4170596 A1, 1979 ;
反应条件
maleic anhydride; trimethylsilyl iodide in acetonitrile Ambient temperature;
参考文献
Synthetic Communications, , vol. 20, # 12 p. 1877 - 1884
反应条件
chromium(VI) oxide; sulfuric acid in dichloromethane T=-5°C; 1 h;
参考文献
Reimann; Poschl
Pharmazie, 1995 , vol. 50, # 9 p. 589 - 592
反应条件
Pancreatin; triethylamine in tetrahydrofuran T=20°C; Enzymatic reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 6 p. 357 - 365