1-叔丁基-2,4-二硝基苯合成路线 (共 13 条)
反应条件
cyclohexane; palladium
参考文献
Stegmann,H.B. et al.
Chemische Berichte, 1976 , vol. 109, p. 2243 - 2258
反应条件
1: alcohol; hydrogen sulfide; ammonia 2: absolute-alcoholic sulfuric acid / Diazotization View Scheme
参考文献
Lesslie,M.S.; Mayer,U.J.H.
Journal of the Chemical Society, 1961 , p. 611 - 618
反应条件
1: alcohol; hydrogen sulfide; ammonia 2: absolute-alcoholic sulfuric acid / Diazotization 3: iron; acetic acid / 90 °C View Scheme
参考文献
Lesslie,M.S.; Mayer,U.J.H.
Journal of the Chemical Society, 1961 , p. 611 - 618
反应条件
1: 33.2 g / Na2S*9H2O, sulphur / H2O / 1.5 h / Heating 2: 28.5 g View Scheme
参考文献
Shoesmith; Mackie
Journal of the Chemical Society, 1928 , p. 2336
反应条件
sodium sulfide; sulfur
参考文献
Atwal, Karnail S.; Ferrara, Francis N.; Ding, Charles Z.; Grover, Gary J.; Sleph, Paul G.; Dzwonczyk, Steven; Baird, Anne J.; Normandin, Diane E.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 1 p. 304 - 313
参考文献
Shoesmith; Mackie
Journal of the Chemical Society, 1928 , p. 2336
反应条件
1: 86 percent / aq. sodium sulfide, sulfur 2: 1.) conc. HCl, aq. NaNO2, 2.) aq. KCN / 1.) EtOH, 0 deg C, 10 min, 2.) EtOH, 100 deg C, 15 min 3: SnCl2*2H2O / ethanol / 0.75 h / Heating View Scheme
参考文献
Atwal, Karnail S.; Ferrara, Francis N.; Ding, Charles Z.; Grover, Gary J.; Sleph, Paul G.; Dzwonczyk, Steven; Baird, Anne J.; Normandin, Diane E.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 1 p. 304 - 313
反应条件
sulfuric acid; nitric acid
T=0 - 20°C;
参考文献
Dangel, Brian D.; Godula, Kamil; Youn, So Won; Sezen, Bengue; Sames, Dalibor
Journal of the American Chemical Society, 2002 , vol. 124, # 40 p. 11856 - 11857
参考文献
Shoesmith; Mackie
Journal of the Chemical Society, 1928 , p. 2336
反应条件
trinitratooxovanadium(V) in dichloromethane
0.05 h; Ambient temperature;
参考文献
Dove, Michael F. A.; Manz, Berthold; Montgomery, John; Pattenden, Gerald; Wood, Simon A.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 10 p. 1589 - 1590