2-(4-甲氧基苄氧基)噻吩合成路线 (共 23 条)
反应条件
iron(III) oxide T=20°C; Friedel Crafts acylation; 0.333333 h; regioselective reaction;
参考文献
Sharghi, Hashem; Jokar, Mahboubeh; Doroodmand, Mohammad Mahdi; Khalifeh, Reza
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 3031 - 3044
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in various solvent(s) T=80°C; P=760 Torr; 5 h;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
反应条件
caesium carbonate; palladium dichloride in acetonitrile T=20°C; Substitution; 3 h;
参考文献
Kang, Suk-Ku; Lee, Sang-Woo; Ryu, Hyung-Chul
Chemical Communications, 1999 , # 20 p. 2117 - 2118
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
反应条件
tin(IV) chloride in dichloromethane T=23°C; Friedel-Crafts reaction; 5 h;
参考文献
Zhao, Weili; Carreira, Erick M.
Chemistry - A European Journal, 2007 , vol. 13, # 9 p. 2671 - 2688
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in methoxybenzene T=100°C; Suzuki carbonylative coupling; P=760.051 Torr; 20 h; chemoselective reaction;
参考文献
Li, Hongling; Yang, Min; Qi, Yanxing; Xue, Jijun
European Journal of Organic Chemistry, 2011 , # 14 p. 2662 - 2667
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; potassium iodide in various solvent(s) T=80°C; P=760 Torr; 16 h;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
反应条件
water; palladium dichloride in ethylene glycol dimethyl ether 0.333333 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Ho, Pil-Su; Yoon, Seok-Keun; Lee, Ju-Cheol; Lee, Kyung-Ju
Synthesis, 1998 , # 6 p. 823 - 825
反应条件
palladium diacetate; potassium carbonate in methoxybenzene T=140°C; Suzuki coupling; 12 h;
参考文献
Jafarpour, Farnaz; Rashidi-Ranjbar, Parviz.; Kashani, Asieh Otaredi
European Journal of Organic Chemistry, 2011 , # 11 p. 2128 - 2132
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethylene glycol dimethyl ether P=760 Torr; 1 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Lim, Kwon-Ho; Ho, Pil-Su; Yoon, Seok-Keun; Son, Hoe-Joo
Synthetic Communications, 1998 , vol. 28, # 8 p. 1481 - 1489