(2-甲氧基苯甲酰)乙酸乙酯合成路线 (共 19 条)
反应条件
sodium; ethyl acetate
参考文献
Kindler; Peschke
Archiv der Pharmazie (Weinheim, Germany), 1933 , vol. 271, p. 431,435
参考文献
Tahara
Chemische Berichte, 1892 , vol. 25, p. 1304
反应条件
hydroxylamine hydrochloride in acetic acid 1 h; Heating;
参考文献
Chantegrel, Bernard; Nadi, Abdel Ilah; Gelin, Suzanne
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4419 - 4424
参考文献
Tahara
Chemische Berichte, 1892 , vol. 25, p. 1304
参考文献
Tahara
Chemische Berichte, 1892 , vol. 25, p. 1304
反应条件
sulfuric acid; water
参考文献
v. Kostanecki; Szabranski
Chemische Berichte, 1904 , vol. 37, p. 2635
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Tahara
Chemische Berichte, 1892 , vol. 25, p. 1304
Full Text Show Details
Edelstein; v. Kostanecki
Chemische Berichte, 1905 , vol. 38, p. 1508
反应条件
sulfuric acid; palladium; acetic acid
Hydrogenation;
参考文献
Kindler; Peschke
Archiv der Pharmazie (Weinheim, Germany), 1933 , vol. 271, p. 431,435
反应条件
1: 75 percent / MsN3 / acetonitrile / 3 h / 30 °C
2: 65 percent / Rh2(OAc)4 / benzene / 0.5 h / Heating
View Scheme
参考文献
Karche; Jachak; Dhavale
Journal of Organic Chemistry, 2001 , vol. 66, # 19 p. 6323 - 6332
反应条件
1: anhydrous iron chloride; di-tert-butyl peroxide; [2,2']bipyridinyl / 1,2-dichloro-ethane / 8 h / 70 °C / |Inert atmosphere
2: boron tribromide / dichloromethane / 0 - 20 °C / |Inert atmosphere
3: ethanol / |Reflux
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参考文献
Kshirsagar, Umesh A.; Parnes, Regev; Goldshtein, Hagit; Ofir, Rivka; Zarivach, Raz; Pappo, Doron
Chemistry - A European Journal, 2013 , vol. 19, # 40 p. 13575 - 13583