2,4-二甲基-1,4-戊二烯合成路线 （共 14 条）
反应条件
sodium tetrahydroborate; Hg(NO3)2 Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bloodworth, A. J.; Khan, Jamil A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2450 - 2457
反应条件
lithium borohydride; Et3CoLi; ethyl acetate
参考文献
Brown, Herbert C.; Somayaji, Vishwanatha; Narasimhan, S.
Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 4822 - 4827
反应条件
mercury Irradiation;
参考文献
Srinivasan,R.; Carlough,K.H.
Journal of the American Chemical Society, 1967 , vol. 89, p. 4932 - 4936
反应条件
mercury Irradiation;
参考文献
Srinivasan,R.; Carlough,K.H.
Journal of the American Chemical Society, 1967 , vol. 89, p. 4932 - 4936
反应条件
tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide
electrochemical reduction;
参考文献
Zefirov, N. S.; Lukin, K. A.; Kozhushkov, S. I.; Kuznetsova, T. S.; Domarev, A. M.; Sosonkin, I. M.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 2.1 p. 278 - 284
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 2 p. 312 - 319
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium in diethyl ether
T=-10°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Zefirov, N. S.; Lukin, K. A.; Kozhushkov, S. I.; Kuznetsova, T. S.; Domarev, A. M.; Sosonkin, I. M.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 2.1 p. 278 - 284
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 2 p. 312 - 319
反应条件
boron trifluoride diethyl etherate
T=0 - 25°C; nachfolgendes Destillieren;
参考文献
Eastman Kodak Co.
Patent: US2450133 , 1947 ;
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Eastman Kodak Co.
Patent: US2462357 , 1948 ;
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Eastman Kodak Co.
Patent: US2450134 , 1947 ;
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Eastman Kodak Co.
Patent: US2450118 , 1947 ;
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Eastman Kodak Co.
Patent: US2450116 , 1947 ;
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Eastman Kodak Co.
Patent: US2450117 , 1947 ;
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Hagemeyer
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 769
Full Text Show Details
Eastman Kodak Co.
Patent: US2450132 , 1947 ;
Full Text Show Details
Eastman Kodak Co.
Patent: US2450131 , 1947 ;
反应条件
tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide
electrochemical reduction; Yield given. Yields of byproduct given;
参考文献
Zefirov, N. S.; Lukin, K. A.; Kozhushkov, S. I.; Kuznetsova, T. S.; Domarev, A. M.; Sosonkin, I. M.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 2.1 p. 278 - 284
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 2 p. 312 - 319
反应条件
1: phosphorus (III)-bromide
2: diethyl ether / Erwaermen des nach Abdestillieren des Loesungmittels erhaltenen Reaktionsgemisches auf 60-70grad
View Scheme
参考文献
Tschel'zowa et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 522,526; engl.Ausg.S. 459, 462
反应条件
diethyl ether
Erwaermen des nach Abdestillieren des Loesungsmittels erhaltenen Reaktionsgemisches auf 60-70grad;
参考文献
Tschel'zowa et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 522,526; engl.Ausg.S. 459, 462
