2,4,5-三氯硫代苯甲醚合成路线 (共 5 条)
反应条件
tetramethylstannane; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 4 h;
参考文献
Cochran, John C.; Friedman, Susan R.; Frazier, John P.
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1533 - 1536
反应条件
1: 81 percent / chlorine, iodine / CCl4 2: tetramethylstannane / tetrakis(triphenylphosphine)palladium(0) / tetrahydrofuran / 4 h / 25 °C View Scheme
参考文献
Pilgram,K.; Korte,F.
Tetrahedron, 1965 , vol. 21, p. 1999 - 2013
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 4 h; Yields of byproduct given;
参考文献
Cochran, John C.; Friedman, Susan R.; Frazier, John P.
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1533 - 1536
参考文献
Pilgram,K.; Korte,F.
Tetrahedron, 1965 , vol. 21, p. 1999 - 2013
反应条件
dihydrogen peroxide; acetic anhydride; acetic acid
参考文献
Pilgram,K.; Korte,F.
Tetrahedron, 1965 , vol. 21, p. 1999 - 2013