反应条件
n-butyllithium; sulfur
1.) hexane, diethyl ether, reflux, 2 h then room t., 15 h; 2.) thf, 2 h, room t. then room t., 15 h; Yield given. Multistep reaction;
参考文献
Dupont, Jairton; Beydoun, Nohma; Pfeffer, Michel
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1715 - 1720