1,1-二甲氧基-2-甲基丙烷合成路线 (共 28 条)
反应条件
methanol; phosphoric acid
T=60 - 80°C;
参考文献
Nasarow et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 106,109; engl. Ausg. S. 111, 112
反应条件
KU-2 ion exchange resin in toluene
T=40°C; 10 h; H2SO4; Product distribution;
参考文献
Musavirov, R. S.; Gazizova, L. B.; Nedogrei, E. P.; Kantor, E. A.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 5 p. 1066 - 1070,889 - 892
参考文献
Teuscher
Journal of the American Chemical Society, 1950 , vol. 72, p. 4316
参考文献
Teuscher
Journal of the American Chemical Society, 1950 , vol. 72, p. 4316
参考文献
Universal Oil Prod. Co.
Patent: US2412012 , 1944 ;
反应条件
water; toluene-4-sulfonic acid; triethylamine
T=90°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
Kyowa Hakko Chemical Co., Ltd.
Patent: EP1876163 A1, 2008 ;
Location in patent: Page/Page column 4 ;
参考文献
Gosselin, Pascal; Rouessac, Francis; Zamarlik, Henri
Bulletin de la Societe Chimique de France, 1981 , vol. 2, # 5-6 p. 192 - 198
反应条件
water; toluene-4-sulfonic acid; triethylamine
T=90°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
Kyowa Hakko Chemical Co., Ltd.
Patent: EP1876163 A1, 2008 ;
Location in patent: Page/Page column 4-5 ;
反应条件
KU-2 ion exchange resin
T=20°C; 8 h;
参考文献
Musavirov, R. S.; Gazizova, L. B.; Nedogrei, E. P.; Kantor, E. A.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 5 p. 1066 - 1070,889 - 892
反应条件
1: 62 percent / p-toluenesulfonic acid / Heating
2: 80 percent / potassium t-butoxide / pentane / 1.) 0 deg C, 1.5 h, 2.) RT, 10 h
View Scheme
参考文献
Hamon, David P. G.; Trenerry, Craige V.
Australian Journal of Chemistry, 1980 , vol. 33, # 4 p. 809 - 821