1,1-二甲氧基-2-甲基丙烷合成路线 （共 28 条）
反应条件
1: 39 percent / p-TsOH / Heating
2: 60 percent / t-BuOK / dimethylsulfoxide
3: 63 percent / p-TsOH / Heating
View Scheme
参考文献
Taskinen, Esko
Magnetic Resonance in Chemistry, 1997 , vol. 35, # 2 p. 107 - 110
反应条件
hydrogenchloride; zinc(II) chloride
1.) ethyl acetate, room temp.; Yield given. Multistep reaction;
参考文献
Makin, S. M.; Kruglikova, R. I.; Tagirov, T. K.; Kharitonova, O. V.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 6 p. 1075 - 1078
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1182 - 1185
反应条件
zinc(II) chloride in ethyl acetate
Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Makin, S. M.; Kruglikova, R. I.; Tagirov, T. K.; Kharitonova, O. V.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 6 p. 1075 - 1078
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1182 - 1185
反应条件
titanium tetrachloride in dichloromethane
1.) -50 deg C, 2.) 3 h room temperature;
参考文献
Pellissier, Helene; Meou, Alain; Gil, Gerard
Tetrahedron Letters, 1986 , vol. 27, # 26 p. 2979 - 2980
反应条件
thionyl chloride; acetyl chloride
参考文献
Kwart,H.; Silver,P.A.
Journal of Organic Chemistry, 1975 , vol. 40, p. 3019 - 3026
反应条件
toluene-4-sulfonic acid
Heating;
参考文献
Taskinen, Esko
Magnetic Resonance in Chemistry, 1997 , vol. 35, # 2 p. 107 - 110
反应条件
toluene-4-sulfonic acid
P=15 Torr; 24 h; Ambient temperature;
参考文献
Frauenrath, Herbert; Runsink, Jan
Journal of Organic Chemistry, 1987 , vol. 52, # 13 p. 2707 - 2712
反应条件
titanium tetrachloride in dichloromethane
参考文献
Mukaiyama,T. et al.
Chemistry Letters, 1974 , p. 323 - 326
