5-甲基-4-氧代-己酸合成路线 (共 18 条)
反应条件
hydrogen; palladium on activated charcoal in water; acetic acid P=570 - 760 Torr; 2 h;
参考文献
Feuer, Henry; Scholl, Philip C.
Heterocycles, 1982 , vol. 18, p. 29 - 35
反应条件
iron (III) acetylacetonate in tetrahydrofuran; diethyl ether T=0°C;
参考文献
Barberis, Mario; Perez-Prieto, Julia
Tetrahedron Letters, 2003 , vol. 44, # 35 p. 6683 - 6685
反应条件
1: 3-methyl-2-morpholin-4-yl-butyronitrile With sodium hydride in N,N-dimethyl-formamide T=0°C; 0.5 h; 2: acrylic acid methyl ester in N,N-dimethyl-formamide T=0 - 20°C;
参考文献
Pawar; Waghmare; Lokhande
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 11 p. 2549 - 2551
反应条件
hydrogenchloride; water 1 h; Heating;
参考文献
Schick, Hans; Ludwig, Ralf
Synthesis, 1992 , # 4 p. 369 - 370
反应条件
hydrogenchloride 0.5 h; Heating;
参考文献
Feuer, Henry; Scholl, Philip C.
Heterocycles, 1982 , vol. 18, p. 29 - 35
反应条件
1: 85 percent / Cu / 1 h / 95 °C 2: 85 percent / aq. KOH / ethanol / 1 h / Heating 3: methanol; H2O / 0.5 h / Heating View Scheme
参考文献
Kunz, Horst; Lindig, Markus
Chemische Berichte, 1983 , vol. 116, # 1 p. 220 - 229
反应条件
1: 85 percent / aq. KOH / ethanol / 1 h / Heating 2: methanol; H2O / 0.5 h / Heating View Scheme
参考文献
Kunz, Horst; Lindig, Markus
Chemische Berichte, 1983 , vol. 116, # 1 p. 220 - 229
参考文献
Linstead; Rydon
Journal of the Chemical Society, 1933 , p. 583
Full Text Show Details
Spassoff
Bulletin de la Societe Chimique de France, 1937 , vol. <5> 4, p. 1658,1659
反应条件
alkaline bromine solution
参考文献
Tiemann; Semmler
Chemische Berichte, 1897 , vol. 30, p. 439
Chemische Berichte, 1898 , vol. 31, p. 2311
反应条件
potassium permanganate Oxydation;
参考文献
Tiemann; Semmler
Chemische Berichte, 1898 , vol. 31, p. 2312