5-甲基-4-氧代-己酸合成路线 （共 18 条）
反应条件
in methanol; water 0.5 h; Heating; Yield given;
参考文献
Kunz, Horst; Lindig, Markus
Chemische Berichte, 1983 , vol. 116, # 1 p. 220 - 229
反应条件
1: 2: With hydrogenchloride
参考文献
Duke University
Patent: US6359182 B1, 2002 ;
Location in patent: Page column 54 ;
反应条件
bei folgender Verseifung;
参考文献
Ivanoff; Spassoff
Bulletin de la Societe Chimique de France, 1934 , vol. <5>1, p. 1421
Full Text Show Details
Spassoff
Bulletin de la Societe Chimique de France, 1937 , vol. <5> 4, p. 1658,1659
反应条件
β-thujadicarboxylic acid (higher-melting form);
参考文献
Ranta
Suomen Kemistilehti B, 1938 , vol. 11, p. 8
Chem. Zentralbl., 1938 , vol. 109, # II p. 2122
反应条件
hydrazine in ethanol 3 h; Heating / reflux;
参考文献
Sumitomo Chemical Takeda Agro Company, Limited
Patent: EP1466527 A1, 2004 ;
Location in patent: Page 23 ;
反应条件
sulfuric acid T=20°C;
参考文献
Guijarro, David; Pablo, Oscar; Yus, Miguel
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3647 - 3654
反应条件
1: 98 percent / DCC; 4-pyrrolidin-1-ylpyridine / CH2Cl2 / 1 h / 20 °C
2: MgBr2*OEt2 / CH2Cl2; diethyl ether / 5 h / -78 °C
View Scheme
参考文献
Tamai, Yasufumi; Hattori, Tetsutaro; Date, Masamitsu; Koike, Shinji; Kamikubo, Yoshinori; Akiyama, Masahiro; Seino, Kazuhiro; Takayama, Hideki; Oyama, Tomohito; Miyano, Sotaro
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1685 - 1694
反应条件
hydrogenchloride; sodium amalgam; water
参考文献
Linstead; Rydon
Journal of the Chemical Society, 1933 , p. 583
Full Text Show Details
Birkinshaw; Oxford; Raistrick
Biochemical Journal, 1936 , vol. 30, p. 407
