暂无反应条件数据

1: 90 h / 100 °C 2: SOCl2 / 14 h / Ambient temperature 3: 83 percent / SnCl4 / CH2Cl2 / 1.)0 deg C, 2.)R.T., 16 h 4: 90 percent / 85percent hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / Heating 5: 67 percent / Raney nickel, 10percent Na2CO3 / ethanol / 16 h / Heating 6: 96 percent / diethyl ether / 12 h / 0 °C 7: 1.)thallium(III) trifluoroacetate, trifluoracetic acid, 2.)isomayl nitrite, 12N HCl, AcOH / 1.)r.t., 48 h, 2.)CH2Cl2, red lights, 10 min. 8: 90 percent / NaBH4 / Palladium on charcoal / methanol / 0.5 h / Ambient temperature 9: 1.)0.5N HCl, sodium nitrite / 1.)0-5 deg C, 5 min., 2.)H2O, 0-5 deg C, 20 min. 10: 53 percent / 1N NaOH / ethanol / 1 h / Heating 11: 65 percent / Trifluoroacetic acid, NaI / acetone / 1.)0-5 deg C, 2.)15 min., 25 deg C View Scheme

aluminium trichloride

暂无反应条件数据

in xylene 2 h; Heating;

1: 52 percent / AlCl3 / nitrobenzene / 1) 20 deg C, 3 h, 2) 45 deg C, 1 h 2: 50percent hydrobromic acid / H2O / 16 h / Heating 3: p-toluenesulphonic acid / 5 h / Heating 4: 1) Na / 1) methanol, 10 min, 2) DMSO, 100 deg C, 8 h View Scheme

aluminium trichloride in 1,2-dichloro-ethane 1) 20 deg C, 3 h, 2) 45 deg C, 1 h;

1: 47 percent / NaBH4 2: KHMDS / tetrahydrofuran; toluene / 0.17 h / -78 °C 3: (Bu3Sn)(Bu)CuLi*CN / tetrahydrofuran / -78 °C View Scheme

1: 99 percent / 0.75 h / 80 °C 2: 94 percent / SOCl2 View Scheme

1: 44 percent / LiAlH4 / tetrahydrofuran / 2 h / 20 °C 2: 73 percent / PBr3 / 20 h / -10 - 20 °C 3: 89 percent / NaI / acetone / 3 h / Heating View Scheme