4-(2-丙烯基)-2-环己烯-1-酮合成路线 （共 5 条）
反应条件
1: With lithium aluminium tetrahydride in diethyl ether
1 h;
2: With hydrogenchloride in diethyl ether
0.5 h; Further stages.;
参考文献
Huffman, John W.; Thompson, Alicia L.S.; Wiley, Jenny L.; Martin, Billy R.
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 1 p. 322 - 335
反应条件
1: 76 percent / 1 M Et2Zn / diethyl ether; hexane / 2 h / Heating
2: 1.) ferric chloride, 2.) NaOAc / 1.) DMF, 1 h, 2.) MeOH, 3 h, heating
View Scheme
参考文献
Booker-Milburn; Thompson
Tetrahedron, 1995 , vol. 51, # 47 p. 12955 - 12962
反应条件
disodium hydrogenphosphate; sodium amalgam; toluene-4-sulfonic acid
1.) methanol, room temp., 30 min, 2.) ethanol, reflux, 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Paquette, Leo A.; Kinney, William A.
Tetrahedron Letters, 1982 , vol. 23, # 2 p. 131 - 134
反应条件
jones' reagent
1.) 1,2-CH2Cl2, reflux, 15 h; 2.) acetone; Yield given. Multistep reaction;
参考文献
Birch, Arthur J.; Kelly, Lawrence F.; Narula, Acharan S.
Tetrahedron, 1982 , vol. 38, # 12 p. 1813 - 1824
反应条件
1: LDA / -78 °C
2: LiAlH4
View Scheme
参考文献
Cossy, Janine; Furet, Nathalie; BouzBouz, Samir
Tetrahedron, 1995 , vol. 51, # 43 p. 11751 - 11764
